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RESEARCH PAPER · ChemElectroChem · 2017

3D‐Printed Electrodes with Improved Mass Transport Properties

Jonas Lölsberg, Ottokar Starck, Serafin Stiefel, Jonas Hereijgers, Tom Breugelmans, Matthias Weßling

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3D‐Printed Electrodes with Improved Mass Transport PropertiesOriginal3D-printed conductive static mixers enable all-vanadium redox flow battery using slurry electrodes72(Bio)Analytical chemistry enabled by 3D printing: Sensors and biosensors218Indirect 3D Printed Electrode Mixers26Three-dimensional porous metal electrodes: Fabrication, characterisation and use90Developments in plane parallel flow channel cells44Mass transfer and hydrodynamic characterization of structured 3D electrodes for electrochemistry70High-Throughput Production of Micrometer Sized Double Emulsions and Microgel Capsules in Parallelized 3D Printed Microfluidic Devices23Intensifying Diffusion-Limited Reactions by Using Static Mixer Electrodes in a Novel Electrochemical Flow Cell9Additively Manufactured Lead–Zirconate–Titanate Thin Films for Hard-Disk Drive Applications1Critical Review—The Versatile Plane Parallel Electrode Geometry: An Illustrated Review90Electrochemical Engineering Assessment of a Novel 3D-Printed Filter-Press Electrochemical Reactor for Multipurpose Laboratory Applications57Overcoming diffusion limitations in electrochemical microreactors using acoustic streaming7A virtuous cycle in materials engineering and surface finishing: design-print-image9On the Resistances of a Slurry Electrode Vanadium Redox Flow Battery29Emerging trends in flow chemistry enabled by 3D printing: Robust reactors, biocatalysis and electrochemistry50Review—The Design, Performance and Continuing Development of Electrochemical Reactors for Clean Electrosynthesis1403D printing of metal-based materials for renewable energy applications493D Printing Technology in the Environment6One-dimensional analytical model for optimizing porosity distribution of multi-layered electrode in redox flow cells0Design, imaging and performance of 3D printed open‐cell architectures for porous electrodes: quantification of surface area and permeability15Prospects for laser based powder bed fusion in the manufacturing of metal electrodes: A review18A review on additive manufacturing and materials for catalytic applications: Milestones, key concepts, advances and perspectives149Porous PVDF Monoliths with Templated Geometry11Inertially enhanced mass transport using 3D-printed porous flow-through electrodes with periodic lattice structures72Computational design of microarchitected porous electrodes for redox flow batteries623D-printed cobalt-rich tungsten carbide hierarchical electrode for efficient electrochemical ammonia production22Electrochemical oscillatory baffled reactors fabricated with additive manufacturing for efficient continuous-flow oxidations1Additive manufacturing of composite porosity mixer electrodes20Sequential vs integrated CO2 capture and electrochemical conversion: An energy comparison4Recent advances in 3D printing for catalytic applications185Electrochemical oscillatory baffled reactors fabricated with additive manufacturing for efficient continuous-flow oxidations0Electrochemical Oscillatory Baffled Reactors Fabricated with Additive Manufacturing for Efficient Continuous-Flow Oxidations19Continuum Modeling of Porous Electrodes for Electrochemical Synthesis146Accelerated parametrization of catalyst performance in organic electrosynthesis4Direct photo-curing 3D printing of nickel-based electrocatalysts for highly-efficient hydrogen evolution64Manipulating and Optimizing the Hierarchically Porous Electrode Structures for Rapid Mass Transport in Solid Oxide Cells57Energy comparison of sequential and integrated CO2 capture and electrochemical conversion8Effects of Structured 3D Electrodes on the Performance of Redox Flow Batteries8Energy comparison of sequential and integrated CO2 capture and electrochemical conversion158Intensification of catalytic reactors: A synergic effort of Multiscale Modeling, Machine Learning and Additive Manufacturing40Additive Manufacturing of Intertwined Electrode Pairs ‐ Guided Mass Transport with Gyroids7An electrochemical oscillatory flow reactor with pillar array electrodes improving mass transfer in electrosynthesis16Titanium‐Based Static Mixer Electrodes to Improve the Current Density of Slurry Electrodes**5Maximizing Energy Efficiency in Additive Manufacturing: A Review and Framework for Future Research41Investigating Mass Transfer Relationships in Stereolithography 3D Printed Electrodes for Redox Flow Batteries45e–NETmix: A pioneering electrochemical flow reactor with enhanced mass transfer22Enhanced photoelectrochemical water splitting via 3D flow field structure: Unveiling the decisive role of interfacial mass transfer63D-printed pyramid nickel-based electrode enabling directional bubble traffic and electrolyte flow for efficient hydrogen evolution21A review of porous electrode structural parameters and optimization for redox flow batteries25Metal Alloy‐Functionalized 3D‐Printed Electrodes for Nitrate‐to‐Ammonia Conversion in Zinc‐Nitrate Batteries43D printed optimized electrodes for electrochemical flow reactors41Recent advances in electrode optimization of electrochemical energy devices using topology optimization163D nickel electrodes for hybrid battery and electrolysis devices2A New Method for Creating Structured High‐Performance Current Collectors for Electrochemical Applications3All-vanadium redox flow batteries0Electrochemical oxidation of 5-hydroxymethylfurfural with flow electrodes: A novel approach for continuous synthesis of 2,5-furandicarboxylic acid20An Overview of the Advantages of Combining Photo- and Electrooxidation Processes in Actual Wastewater Treatment12A 3D printed, metal-free, carbon-based catalytic electrode for converting CO 2 into syngas7Understanding the Current Distribution and Mass Transport Properties in 3D-Printed Architected Flow-Through Electrodes93D electrode surface engineering via atomic layer deposition of nickel oxide for improved water oxidation performance8Direct Ink Writing of 3D‐Structured All‐Carbon Electrodes with High Electrical Conductivity for (Vanadium) Redox Flow Batteries10Additive Manufacturing of Electrochemical Reactors for Diluted and Disperse Reactants03D printing of customized catalytic electrodes with CoNX coordinations for reduction CO2 into syngas0Influence of substrate materials on electrocatalytic water splitting: Mechanisms, engineering strategies, and future perspectives17Enhancing Bubble Removal in Geometry‐Optimized Electrodes0Effect of pulsatile flow and 3D-printed electrodes on mass transport and pumping power in electrochemical reactors0Engineering Strategies for Stable Electrochemical Decarboxylation of Carboxylic Acid in Zero‐Gap Flow Cells0

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  1. 3D-printed conductive static mixers enable all-vanadium redox flow battery using slurry electrodes

    Journal of Power Sources · 2018-02-17

    Korcan Perçin, Alexandra Rommerskirchen, Robert Sengpiel, Youri Gendel, Matthias Wessling

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  2. (Bio)Analytical chemistry enabled by 3D printing: Sensors and biosensors

    TrAC Trends in Analytical Chemistry · 2018-04-02

    C. Lorena Manzanares‐Palenzuela, Martin Pumera

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  3. Indirect 3D Printed Electrode Mixers

    ChemElectroChem · 2018-10-29

    Jonas Hereijgers, Jonathan Schalck, Jonas Lölsberg, Matthias Weßling, Tom Breugelmans

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  4. Three-dimensional porous metal electrodes: Fabrication, characterisation and use

    Current Opinion in Electrochemistry · 2019-02-14

    Luis F. Arenas, Carlos Ponce de León, Frank C. Walsh

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  5. Developments in plane parallel flow channel cells

    Current Opinion in Electrochemistry · 2019-03-07

    Frank C. Walsh, Luis F. Arenas, Carlos Ponce de León

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  6. Mass transfer and hydrodynamic characterization of structured 3D electrodes for electrochemistry

    Chemical Engineering Journal · 2019-10-28

    Jonas Hereijgers, Jonathan Schalck, Tom Breugelmans

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  7. High-Throughput Production of Micrometer Sized Double Emulsions and Microgel Capsules in Parallelized 3D Printed Microfluidic Devices

    Polymers · 2019-11-15

    Alexander Jans, Jonas Lölsberg, Abdolrahman Omidinia‐Anarkoli, Robin Viermann, Martin Möller, Laura De Laporte, Matthias Weßling, Alexander J. C. Kuehne

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  8. Intensifying Diffusion-Limited Reactions by Using Static Mixer Electrodes in a Novel Electrochemical Flow Cell

    Journal of The Electrochemical Society · 2020-01-04

    Bita Bayatsarmadi, Mike Horne, Theo Rodopoulos, Dayalan Gunasegaram

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  9. Additively Manufactured Lead–Zirconate–Titanate Thin Films for Hard-Disk Drive Applications

    IEEE Transactions on Magnetics · 2020-01-09

    Weiwei Xu, Felippe J. Pavinatto, Guozhong Cao, John Devin MacKenzie, I. Y. Shen

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  10. Critical Review—The Versatile Plane Parallel Electrode Geometry: An Illustrated Review

    Journal of The Electrochemical Society · 2020-01-31

    Luis F. Arenas, Carlos Ponce de León, Frank C. Walsh

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  11. Electrochemical Engineering Assessment of a Novel 3D-Printed Filter-Press Electrochemical Reactor for Multipurpose Laboratory Applications

    ACS Sustainable Chemistry & Engineering · 2020-02-13

    Raúl A. Márquez, Virginia Hidolina Collins-Martínez, Ildebrando Pérez-Reyes, David Chávez‐Flores, Olivia A. Graeve, Víctor H. Ramos-Sánchez

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  12. Overcoming diffusion limitations in electrochemical microreactors using acoustic streaming

    Journal of Flow Chemistry · 2020-02-17

    Senne Fransen, Stefan Ballet, Jan Fransaer, Simon Kuhn

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  13. A virtuous cycle in materials engineering and surface finishing: design-print-image

    Transactions of the IMF · 2020-03-03

    Frank C. Walsh, Luis F. Arenas, Carlos Ponce de León

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  14. On the Resistances of a Slurry Electrode Vanadium Redox Flow Battery

    ChemElectroChem · 2020-04-14

    Korcan Perçin, Bart van der Zee, Matthias Weßling

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  15. Emerging trends in flow chemistry enabled by 3D printing: Robust reactors, biocatalysis and electrochemistry

    Current Opinion in Green and Sustainable Chemistry · 2020-06-18

    Víctor Sans

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  16. Review—The Design, Performance and Continuing Development of Electrochemical Reactors for Clean Electrosynthesis

    Journal of The Electrochemical Society · 2020-10-28

    Samuel Charles Perry, Carlos Ponce de León, Frank C. Walsh

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  17. 3D printing of metal-based materials for renewable energy applications

    Nano Research · 2020-12-04

    Shahryar Mooraj, Zhen Qi, Cheng Yan Zhu, Jie Ren, Siyuan Peng, Liang Liu, Shengbiao Zhang, Shuai Feng, Fanyue Kong, Yanfang Liu, Eric B. Duoss, Sarah E. Baker, Wen Chen

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  18. 3D Printing Technology in the Environment

    Environmental and microbial biotechnology · 2021-01-01

    Célia G. Amorim, Renato L. Gil, Jaime E. Cevallos-Mendoza, Alberto N. Araújo, Joan Manuel Rodríguez-Díaz, Maria C. B. S. M. Montenegro

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  19. One-dimensional analytical model for optimizing porosity distribution of multi-layered electrode in redox flow cells

    Unknown journal · 2021-03-02

    Junyi Tao, Zhichao Chen, Limin Qi, Menglian Zheng

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  20. Design, imaging and performance of 3D printed open‐cell architectures for porous electrodes: quantification of surface area and permeability

    Journal of Chemical Technology & Biotechnology · 2021-04-10

    Nazira Kaishubayeva, Carlos Ponce de León, Frank C. Walsh, Luis F. Arenas

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  21. Prospects for laser based powder bed fusion in the manufacturing of metal electrodes: A review

    Applied Materials Today · 2021-04-24

    Patricia Nyamekye, Pinja Nieminen, Mohammad Reza Bilesan, Eveliina Repo, Heidi Piili, Antti Salminen

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  22. A review on additive manufacturing and materials for catalytic applications: Milestones, key concepts, advances and perspectives

    Materials & Design · 2021-06-22

    O.H. Laguna, Pablo F. Lietor, Francisco Javier Iglesias-Godino, Francisco Antonio Corpas-Iglesias

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  23. Porous PVDF Monoliths with Templated Geometry

    Advanced Materials Technologies · 2021-07-08

    Suzana Djeljadini, Patrick Bongartz, Michael Alders, Nils Hartmann, Alexander Oing, Christian Gabriel Cornelissen, Felix Hesselmann, Jutta Arens, Ulrich Steinseifer, John Linkhorst, Matthias Weßling

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  24. Inertially enhanced mass transport using 3D-printed porous flow-through electrodes with periodic lattice structures

    Proceedings of the National Academy of Sciences · 2021-08-06

    V. A. Beck, Anna N. Ivanovskaya, Swetha Chandrasekaran, Jean‐Baptiste Forien, Sarah E. Baker, Eric B. Duoss, Marcus Andre Worsley

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  25. Computational design of microarchitected porous electrodes for redox flow batteries

    Journal of Power Sources · 2021-09-11

    V. A. Beck, Jonathan J. Wong, Charles F. Jekel, Daniel A. Tortorelli, Sarah E. Baker, Eric B. Duoss, Marcus Andre Worsley

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  26. 3D-printed cobalt-rich tungsten carbide hierarchical electrode for efficient electrochemical ammonia production

    Journal of the Korean Ceramic Society · 2021-10-01

    Dong‐Kyu Lee, Sung-Jun Wee, Kyung-Jun Jang, Mi‐Kyung Han, Subramani Surendran, Sung Yong Cho, Joon‐Young Kim, Sang‐Kyu Lee, Uk Sim

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  27. Electrochemical oscillatory baffled reactors fabricated with additive manufacturing for efficient continuous-flow oxidations

    Unknown journal · 2021-10-05

    Elena Álvarez, María Romero‐Fernández, Diego Iglesias, Raúl Martı́nez-Cuenca, Obinna Okafor, Astrid E. Delorme, Alex v.E. Conradie, Pedro Lozano, Peter Licence, Ruth Goodridge, Sergio Chiva, Francesca Paradisi, Darren A. Walsh, Víctor Sans

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  28. Additive manufacturing of composite porosity mixer electrodes

    Electrochemistry Communications · 2021-12-04

    Alexander Limper, Nils Weber, Anselm Brodersen, Robert Keller, Matthias Weßling, John Linkhorst

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  29. Sequential vs integrated CO2 capture and electrochemical conversion: An energy comparison

    ChemRxiv · 2021-12-17

    Mengran Li, Erdem Irtem, Hugo Pieter Iglesias van Montfort, Thomas Burdyny

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  30. Recent advances in 3D printing for catalytic applications

    Chemical Engineering Journal · 2021-12-27

    Jie Zhu, Peiwen Wu, Yanhong Chao, Jiangtao Yu, Wenshuai Zhu, Zhichang Liu, Chunming Xu

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  31. Electrochemical oscillatory baffled reactors fabricated with additive manufacturing for efficient continuous-flow oxidations

    Unknown journal · 2022-01-12

    Elena Álvarez, María Romero‐Fernández, Diego Iglesias, Raúl Martı́nez-Cuenca, Obinna Okafor, Astrid E. Delorme, Pedro Lozano, Ruth Goodridge, Francesca Paradisi, Darren A. Walsh, Víctor Sans

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  32. Electrochemical Oscillatory Baffled Reactors Fabricated with Additive Manufacturing for Efficient Continuous-Flow Oxidations

    ACS Sustainable Chemistry & Engineering · 2022-02-11

    Elena Álvarez, María Romero‐Fernández, Diego Iglesias, Raúl Martı́nez-Cuenca, Obinna Okafor, Astrid E. Delorme, Alex v.E. Conradie, Pedro Lozano, Peter Licence, Ruth Goodridge, Sergio Chiva, Francesca Paradisi, Darren A. Walsh, Víctor Sans

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  33. Continuum Modeling of Porous Electrodes for Electrochemical Synthesis

    Chemical Reviews · 2022-05-04

    Justin C. Bui, Eric W. Lees, Lalit Mohan Pant, Iryna V. Zenyuk, Alexis T. Bell, Adam Z. Weber

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  34. Accelerated parametrization of catalyst performance in organic electrosynthesis

    Current Opinion in Electrochemistry · 2022-07-07

    Pavlo Nikolaienko, Karl J. J. Mayrhofer

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  35. Direct photo-curing 3D printing of nickel-based electrocatalysts for highly-efficient hydrogen evolution

    Nano Energy · 2022-07-18

    Zhaojing Han, Gang Wang, Jie Zhang, Zhiyong Tang

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  36. Manipulating and Optimizing the Hierarchically Porous Electrode Structures for Rapid Mass Transport in Solid Oxide Cells

    Advanced Functional Materials · 2022-08-19

    Mingyang Hou, Yuxin Pan, Fan He, Kang Xu, Hua Zhang, Yucun Zhou, Bote Zhao, Yu Chen, Meilin Liu

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  37. Energy comparison of sequential and integrated CO2 capture and electrochemical conversion

    ChemRxiv · 2022-08-30

    Mengran Li, Erdem Irtem, Hugo Pieter Iglesias van Montfort, Maryam Abdinejad, Thomas Burdyny

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  38. Effects of Structured 3D Electrodes on the Performance of Redox Flow Batteries

    ChemElectroChem · 2022-09-02

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  39. Energy comparison of sequential and integrated CO2 capture and electrochemical conversion

    Nature Communications · 2022-09-14

    Mengran Li, Erdem Irtem, Hugo‐Pieter Iglesias van Montfort, Maryam Abdinejad, Thomas Burdyny

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  40. Intensification of catalytic reactors: A synergic effort of Multiscale Modeling, Machine Learning and Additive Manufacturing

    Chemical Engineering and Processing - Process Intensification · 2022-09-21

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  41. Additive Manufacturing of Intertwined Electrode Pairs ‐ Guided Mass Transport with Gyroids

    Advanced Engineering Materials · 2022-10-19

    Florian Wiesner, Alexander Limper, Cedric Marth, Anselm Brodersen, Matthias Weßling, John Linkhorst

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  42. An electrochemical oscillatory flow reactor with pillar array electrodes improving mass transfer in electrosynthesis

    Electrochimica Acta · 2022-10-23

    Michiel Vranckaert, Hannes P. L. Gemoets, Ruben Dangreau, Koen Van Aken, Tom Breugelmans, Jonas Hereijgers

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  43. Titanium‐Based Static Mixer Electrodes to Improve the Current Density of Slurry Electrodes**

    ChemElectroChem · 2023-01-10

    Korcan Perçin, Jonas Hereijgers, Nicolas Mulandi, Tom Breugelmans, Matthias Weßling

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  44. Maximizing Energy Efficiency in Additive Manufacturing: A Review and Framework for Future Research

    Energies · 2023-05-18

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  45. Investigating Mass Transfer Relationships in Stereolithography 3D Printed Electrodes for Redox Flow Batteries

    Advanced Materials Technologies · 2023-07-28

    Maxime van der Heijden, Marit Kroese, Zandrie Borneman, Antoni Forner‐Cuenca

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  46. e–NETmix: A pioneering electrochemical flow reactor with enhanced mass transfer

    Chemical Engineering Journal · 2023-12-23

    Daniela F.S. Morais, José Carlos B. Lopes, Madalena M. Dias, Vítor J.P. Vilar, Francisca C. Moreira

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  47. Enhanced photoelectrochemical water splitting via 3D flow field structure: Unveiling the decisive role of interfacial mass transfer

    Process Safety and Environmental Protection · 2024-03-26

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  48. 3D-printed pyramid nickel-based electrode enabling directional bubble traffic and electrolyte flow for efficient hydrogen evolution

    International Journal of Hydrogen Energy · 2024-03-29

    Zhaojing Han, Hao Zhao, Ci Peng, Chuanting Fan, Gang Wang, Jie Zhang, Zhiyong Tang

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  49. A review of porous electrode structural parameters and optimization for redox flow batteries

    Journal of Energy Storage · 2024-07-13

    Pengfei Wang, Yijian Zhao, Yuhang Ban, Menglian Zheng

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  50. Metal Alloy‐Functionalized 3D‐Printed Electrodes for Nitrate‐to‐Ammonia Conversion in Zinc‐Nitrate Batteries

    ChemElectroChem · 2024-07-15

    Si Liu, Yupeng Zhao, Zhengfan Chen, Dandan Gao, Fan Feng, Tobias Rios‐Studer, Joachim Bansmann, Johannes Biskupek, Ute A. Kaiser, Rongji Liu, Carsten Streb

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