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RESEARCH PAPER · Nature Communications · 2017

Understanding materials challenges for rechargeable ion batteries with in situ transmission electron microscopy

Yifei Yuan, Khalil Amine, Jun Biao Lu, Reza Shahbazian‐Yassar

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Understanding materials challenges for rechargeable ion batteries with in situ transmission electron microscopyOriginalIn-situ electron microscopy observation of electrochemical sodium plating and stripping dynamics on carbon nanofiber current collectors72Origin of Fracture‐Resistance to Large Volume Change in Cu‐Substituted Co3O4 Electrodes37Process optimization for producing hierarchical porous bamboo-derived carbon materials with ultrahigh specific surface area for lithium-sulfur batteries66Electron Energy-Loss Spectroscopy and Imaging ☆1Highly efficient and ultra-stable boron-doped graphite felt electrodes for vanadium redox flow batteries144Striping modulations and strain gradients within individual particles of a cathode material upon lithiation23Fundamental Understanding of Nanostructured Si Electrodes: Preparation and Characterization35A Material Perspective of Rechargeable Metallic Lithium Anodes129Advances in Understanding Materials for Rechargeable Lithium Batteries by Atomic Force Microscopy109Encapsulating Various Sulfur Allotropes within Graphene Nanocages for Long‐Lasting Lithium Storage70Developing High‐Performance Lithium Metal Anode in Liquid Electrolytes: Challenges and Progress535One-step nonlinear electrochemical synthesis of TexSy@PANI nanorod materials for Li-TexSy battery33Operando liquid cell electron microscopy of discharge and charge kinetics in lithium-oxygen batteries80Lightning under water: Diverse reactive environments and evidence of synergistic effects for material treatment and activation59Rate-dependent electrochemical reaction mechanism of spinel metal oxide anode studied by in situ TEM10In Situ TEM Investigation of Electron Irradiation Induced Metastable States in Lithium-Ion Battery Cathodes: Li2FeSiO4 versus LiFePO427β-SnSb for Sodium Ion Battery Anodes: Phase Transformations Responsible for Enhanced Cycling Stability Revealed by In Situ TEM107The Design and Synthesis of Hollow Micro‐/Nanostructures: Present and Future Trends393Fe2O3@C core@shell nanotubes: Porous Fe2O3 nanotubes derived from MIL-88A as cores and carbon as shells for high power lithium ion batteries67Molecular polymer-derived ceramics for applications in electrochemical energy storage devices52Low atomic number silicon nitride films for transmission electron microscopy4Metal–Organic Frameworks and Their Derived Materials as Electrocatalysts and Photocatalysts for CO2 Reduction: Progress, Challenges, and Perspectives149Nanostructured Conversion‐Type Negative Electrode Materials for Low‐Cost and High‐Performance Sodium‐Ion Batteries189In Situ Electron Diffraction Tomography Using a Liquid-Electrochemical Transmission Electron Microscopy Cell for Crystal Structure Determination of Cathode Materials for Li-Ion batteries94Improved electrochemical cycling stability of intercalation battery electrodes via control of material morphology9Atomic‐Scale Observation of LiFePO4 and LiCoO2 Dissolution Behavior in Aqueous Solutions55Solid–Liquid Interfacial Reaction Trigged Propagation of Phase Transition from Surface into Bulk Lattice of Ni-Rich Layered Cathode101Reaction: Freezing Electrochemical Interfaces for Robustness in Electron Microscopy6DNA-directed fabrication of NiCo2O4 nanoparticles on carbon nanotubes as electrodes for high-performance battery-like electrochemical capacitive energy storage device100Direct Visualization of Li Dendrite Effect on LiCoO 2 Cathode by In Situ TEM49Enhanced Capacity of NiO Nanocubes with High Dispersion and Exposed Facets Reinforced by Thermal Plasma18Dandelion-shaped manganese sulfide in ether-based electrolyte for enhanced performance sodium-ion batteries59Oxide nanoparticle hybrid materials and applications2The Absence and Importance of Operando Techniques for Metal‐Free Catalysts33Enhanced Lithium Transport by Control of Crystal Orientation in Spinel LiMn2O4 Thin Film Cathodes70A review on density functional theory–based study on two-dimensional materials used in batteries85Addressing Interfacial Issues in Liquid-Based and Solid-State Batteries by Atomic and Molecular Layer Deposition288Status, promises, and challenges of nanocomposite solid-state electrolytes for safe and high performance lithium batteries280Strategies for Building Robust Traffic Networks in Advanced Energy Storage Devices: A Focus on Composite Electrodes96Advanced cathode materials and efficient electrolytes for rechargeable batteries: practical challenges and future perspectives56Characterizing multiple continuous phase transitions at an alloying anode with voltammetric measurements and first-principles calculations6Electron microscopy and its role in advanced lithium-ion battery research35Exploring the charge reactions in a Li–O 2 system with lithium oxide cathodes and nonaqueous electrolytes11High-Energy All-Solid-State Lithium-Metal Batteries by Nanomaterial Designs3In situ observation of lithium metal plating in a sulfur-based solid electrolyte for all-solid-state batteries64Metal–organic framework derived 3D graphene decorated NaTi 2 (PO 4 ) 3 for fast Na-ion storage28Probing the dynamic evolution of lithium dendrites: a review of in situ / operando characterization for lithium metallic batteries34Tailoring natural layered β-phase antimony into few layer antimonene for Li storage with high rate capabilities63Size-dependent kinetics during non-equilibrium lithiation of nano-sized zinc ferrite59Encapsulating phosphorus inside carbon nanotubes via a solution approach for advanced lithium ion host39Interphase Morphology between a Solid-State Electrolyte and Lithium Controls Cell Failure231Single atomic Ag enhances the bifunctional activity and cycling stability of MnO2112A novel metal-organic layered material with superior supercapacitive performance through ultrafast and reversible tetraethylammonium intercalation34Bridging the academic and industrial metrics for next-generation practical batteries611Fabrication of SnS 2 /Mn 2 SnS 4 /Carbon Heterostructures for Sodium-Ion Batteries with High Initial Coulombic Efficiency and Cycling Stability262Advances in Graphene‐Based Liquid Cell Electron Microscopy: Working Principles, Opportunities, and Challenges57The development of 2D materials for electrochemical energy applications: A mechanistic approach33Energetics and cathode voltages of LiMPO4 olivines ( M=Fe , Mn) from extended Hubbard functionals68Graphene Wrapped FeSe 2 Nano‐Microspheres with High Pseudocapacitive Contribution for Enhanced Na‐Ion Storage283Three-dimensional ordered porous electrode materials for electrochemical energy storage327TEM Studies on Electrode Materials for Secondary Ion Batteries2Spot the difference at the nanoscale: identical location electron microscopy in electrocatalysis80Polypyrrole-Coated Sodium Manganate Hollow Microspheres as a Superior Cathode for Sodium Ion Batteries86Interpreting Electrochemical and Chemical Sodiation Mechanisms and Kinetics in Tin Antimony Battery Anodes Using in Situ Transmission Electron Microscopy and Computational Methods16In Situ TEM of Phosphorus-Dopant-Induced Nanopore Formation in Delithiated Silicon Nanowires13Deciphering the Atomic Patterns Leading to MnO2 Polymorphism94Electrochemically primed functional redox mediator generator from the decomposition of solid state electrolyte65The rise of bio-inspired energy devices38Mechanistic understanding and strategies to design interfaces of solid electrolytes: insights gained from transmission electron microscopy18Molybdenum Nitride Nanocrystals Anchored on Phosphorus-Incorporated Carbon Fabric as a Negative Electrode for High-Performance Asymmetric Pseudocapacitor51Atomic-scale combination of germanium-zinc nanofibers for structural and electrochemical evolution54In Situ Transmission Electron Microscopy for Energy Materials and Devices169Structural, microstructural and electrochemical studies of TiO2–Ag double layer coated NCM cathode for lithium-ion batteries10Understanding Challenges of Cathode Materials for Sodium‐Ion Batteries using Synchrotron‐Based X‐Ray Absorption Spectroscopy34Expanded lithiation of titanium disulfide: Reaction kinetics of multi-step conversion reaction25Role of operando microscopy techniques on the advancement of sustainable sodium-ion battery anodes24Unraveling the Origins of the “Unreactive Core” in Conversion Electrodes to Trigger High Sodium-Ion Electrochemistry38Lithiation-Induced Structural Rearrangement and Stress Change in SiCO-Derived Porous Carbon: A First-Principles Study3“Seeing” the Weak Bonding1In Situ Electron Microscopy for Electrically Induced Charge Transport and Phase Transformation0Structure solution and refinement of metal-ion battery cathode materials using electron diffraction tomography13A Game Changer: Functional Nano/Micromaterials for Smart Rechargeable Batteries69A Cell for Controllable Formation and In Operando Electrochemical Characterization of Intercalation Materials for Aqueous Metal‐Ion Batteries6Toward Electrochemical Studies on the Nanometer and Atomic Scales: Progress, Challenges, and Opportunities57Demanding energy from carbon134Interface-Engineering for All-Oxide Solid-State Batteries0Self-Assembled Nanoparticle Supertubes as Robust Platform for Revealing Long-Term, Multiscale Lithiation Evolution60Bibliography0Nanowires for Electrochemical Energy Storage436Recent Progress of In Situ Transmission Electron Microscopy for Energy Materials123Atomistic and dynamic structural characterizations in low-dimensional materials: recent applications of in situ transmission electron microscopy6Morphological and Structural Evolution of Co3O4 Nanoparticles Revealed by in Situ Electrochemical Transmission Electron Microscopy during Electrocatalytic Water Oxidation241Electrochemical Behavior of Carbon Electrodes for In Situ Redox Studies in a Transmission Electron Microscope17Selective Growth of a Discontinuous Subnanometer Pd Film on Carbon Defects for Li–O2 Batteries65Electrochemical and Structural Analysis in All‐Solid‐State Lithium Batteries by Analytical Electron Microscopy: Progress and Perspectives42In-Situ Arc Discharge-Derived FeSn2/Onion-Like Carbon Nanocapsules as Improved Stannide-Based Electrocatalytic Anode Materials for Lithium-Ion Batteries10Advanced Characterizations of Solid Electrolyte Interphases in Lithium-Ion Batteries162In situ TEM investigation of electron beam-induced ultrafast chemical lithiation for charging16Hybrid Electrode Innovations in Triple and Quadruple Dimensions for Lithium‐Ion Batteries9Boosting Superior Lithium Storage Performance of Alloy‐Based Anode Materials via Ultraconformal Sb Coating–Derived Favorable Solid‐Electrolyte Interphase38Phosphorous/oxygen co-doped mesoporous carbon bowls as sulfur host for high performance lithium-sulfur batteries36Understanding Transformations in Battery Materials Using in Situ and Operando Experiments: Progress and Outlook115Advance in interface and characterizations of sulfide solid electrolyte materials32Cationic and anionic redox in lithium-ion based batteries235Mechanoelectrochemical issues involved in current lithium-ion batteries19Operando vibrational spectroscopy for electrochemical biomass valorization38Operando Acoustic Monitoring of SEI Formation and Long-Term Cycling in NMC/SiGr Composite Pouch Cells66Review—Interfaces: Key Issue to Be Solved for All Solid-State Lithium Battery Technologies141α-MoO3 sheets with high exposed plane reinforced by thermal plasma for stable Li-ion storage25Investigating the Effects of Lithium Deposition on the Abuse Response of Lithium-Ion Batteries10Lithium-Gold Reference Electrode for Potential Stability During In Situ Electron Microscopy Studies of Lithium-Ion Batteries21Low-crystalline FeOx@PPy hybridized with (Ni0.25Mn0.75)3O4@PPy to constructed high-voltage aqueous hybrid capacitor with 2.4 V2Li metal deposition and stripping in a solid-state battery via Coble creep500Design strategies for nonaqueous multivalent-ion and monovalent-ion battery anodes437Switchable encapsulation of polysulfides in the transition between sulfur and lithium sulfide143Solution Blowing Synthesis of Li-Conductive Ceramic Nanofibers27Rooting binder-free tin nanoarrays into copper substrate via tin-copper alloying for robust energy storage106Chemical Properties of Lithium Cluster (Lix, x = 2–8) on Stone–Wales Defect Graphene Sheet: A DFT Study15Advanced Matrixes for Binder‐Free Nanostructured Electrodes in Lithium‐Ion Batteries184Surface Amorphization of Vanadium Dioxide (B) for K‐Ion Battery144Recent advances and prospects of layered transition metal oxide cathodes for sodium-ion batteries317From Sodium–Oxygen to Sodium–Air Battery: Enabled by Sodium Peroxide Dihydrate53Probing electrochemical surface/interfacial reactions with liquid cell transmission electron microscopy: a challenge or an opportunity?11Red-phosphorus-impregnated carbon nanofibers for sodium-ion batteries and liquefaction of red phosphorus140Symmetry-Induced Emergent Electrochemical Properties for Rechargeable Batteries8Visualization of Lithium Transfer Resistance in Secondary Particle Cathodes of Bulk-Type Solid-State Batteries74Charge/discharge cycling of Li 1+x (Ni 0.6 Co 0.2 Mn 0.2 ) 1−x O 2 primary particles performed in a liquid microcell for transmission electron microscopy studies14Three-Dimensional Microbatteries beyond Lithium Ion134In Situ TEM Study on Conversion‐Type Electrodes for Rechargeable Ion Batteries104Operando Electrochemical Atomic Force Microscopy of Solid–Electrolyte Interphase Formation on Graphite Anodes: The Evolution of SEI Morphology and Mechanical Properties134Reaction mechanism and structural evolution of fluorographite cathodes in Li/Na/K batteries0TEM Studies on the Role of Local Chemistry and Atomic Structure in Battery Materials0Sulfur-based cathodes operated at strict cycling conditions for Li-based batteries0Seeing is Believing: In Situ/Operando Optical Microscopy for Probing Electrochemical Energy Systems60Polycation ionic liquid tailored PEO-based solid polymer electrolytes for high temperature lithium metal batteries139Regulating the Performance of Lithium-Ion Battery Focus on the Electrode-Electrolyte Interface39Defect and structural evolution under high-energy ion irradiation informs battery materials design for extreme environments65In Situ Atomic‐Scale Observation of Reversible Potassium Storage in Sb 2 S 3 @Carbon Nanowire Anodes103Accessing Lithium–Oxygen Battery Discharge Products in Their Native Environments via Transmission Electron Microscopy Grid Electrode7Surface Modification of Li‐Rich Mn‐Based Layered Oxide Cathodes: Challenges, Materials, Methods, and Characterization193Toward High-Capacity Battery Anode Materials: Chemistry and Mechanics Intertwined43An experimental control system for electron spectrometers using Arduino and LabVIEW interfaces17Rosa roxburghii-like hierarchical hollow sandwich-structure C@Fe2O3@C microspheres as second nanomaterialsfor superior lithium storage41MnS@N,S Co‐Doped Carbon Core/Shell Nanocubes: Sulfur‐Bridged Bonds Enhanced Na‐Storage Properties Revealed by In Situ Raman Spectroscopy and Transmission Electron Microscopy78Probing Lithium Metals in Batteries by Advanced Characterization and Analysis Tools52Beyond Volume Variation: Anisotropic and Protrusive Lithiation in Bismuth Nanowire29Understanding all solid-state lithium batteries through in situ transmission electron microscopy117Current state-of-the-art characterization techniques for probing the layered oxide cathode materials of sodium-ion batteries107In-situ/operando characterization techniques in lithium-ion batteries and beyond130A Low‐Swelling Polymeric Mixed Conductor Operating in Aqueous Electrolytes64

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  50. Encapsulating phosphorus inside carbon nanotubes via a solution approach for advanced lithium ion host

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