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RESEARCH PAPER · Inorganic Chemistry · 2015

Synthesis and Structural Studies of Nickel(0) Tetracarbene Complexes with the Introduction of a New Four-Coordinate Geometric Index, τ δ

Mark H. Reineke, Matthew D. Sampson, Arnold L. Rheingold, Clifford P. Kubiak

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Synthesis and Structural Studies of Nickel(0) Tetracarbene Complexes with the Introduction of a New Four-Coordinate Geometric Index, τ δOriginalIntroducing a pyrazole/imidazole based hybrid cyclophane: a hydrogen bond sensor and binucleating ligand precursor43Structural classification of metal complexes with three-coordinate centres22Structural diversity of late transition metal complexes with flexible tetra-NHC ligands55Probing the Limits of Tetraazamacrocycle‐Glyoxal Condensates as Bidentate Ligands for Cu2+1Supramolecular Assembly of Metal‐Organic Tubes Constructed from the Ditopic Heteroscorpionate Ligand (4‐NH2C6H4)CHpz2 (pz = Pyrazol‐1‐yl) and Silver(I)12Oxygen Activation by Co(II) and a Redox Non-Innocent Ligand: Spectroscopic Characterization of a Radical–Co(II)–Superoxide Complex with Divergent Catalytic Reactivity90Structural comparison of suberanilohydroxamic acid (SAHA) and other zinc-enzyme inhibitors bound to a monomeric zinc species4A mixed valence zinc dithiolene system with spectator metal and reactor ligands12Nickel Complexes of Pyridine‐Functionalized N‐Heterocyclic Carbenes: Syntheses, Structures, and Activity in Electrocatalytic Hydrogen Production21Synthesis and structural characterization of tris(pyrazolyl)hydroaluminate and tris(pyrazolyl)hydrogallate lithium compounds16A hybrid carbocyclic/N-heterocyclic carbene ligand11Silica-supported isolated gallium sites as highly active, selective and stable propane dehydrogenation catalysts166Tris[(1-isopropylbenzimidazol-2-yl)dimethylsilyl]methyl metal complexes, [Tism PriBenz ]M: a new class of metallacarbatranes, isomerization to a tris(N-heterocyclic carbene) derivative, and evidence for an inverted ligand field32Multidentate N-heterocyclic carbene complexes of the 3d metals: Synthesis, structure, reactivity and catalysis164Nickel mediated negishi and oxidative couplings0Tris(2-mercaptoimidazolyl)hydroborato Cadmium Thiolate Complexes, [TmBut]CdSAr: Thiolate Exchange at Cadmium in a Sulfur-Rich Coordination Environment11Stoichiometric and Catalytic Reactivity of Ni(6-Mes)(PPh3)243Gold(III) Bis(di-N-heterocyclic carbene) Square Planar Trication with Axial Ligand Interactions with Bromides from Ag/Br Counteranion Assemblies13Understanding the Lewis Acidity of Co(II) Sites on a Silica Surface17Synthesis and Characterization of Bidentate NHC-CAryl Nickel(II) Complexes: Isocyanide Insertion To Form NHC-η2-iminoacyl Complexes9Role of Coordination Number, Geometry, and Local Disorder on 27Al NMR Chemical Shifts and Quadrupolar Coupling Constants: Case Study with Aluminosilicates44Dinuclear Nickel Complexes of Thiolate-Functionalized Carbene Ligands and Their Electrochemical Properties28Dimerization of a mixed-carbene PdII dibromide complex by elemental iodine2Zerovalent Nickel Compounds Supported by 1,2-Bis(diphenylphosphino)benzene: Synthesis, Structures, and Catalytic Properties23Synthesis and Characterization of Heteroleptic Ni(II) Bipyridine Complexes Bearing Bis(N-heterocyclic carbene) Ligands20Reaction Chemistry of Silver(I) Trifluoromethanesulfonate Complexes of Nitrogen-Confused C-Scorpionates15Can pendant pyridyl arm assist the proton delivery in electrocatalysis?4Elucidating the Solution-Phase Structure and Behavior of 8-Hydroxyquinoline Zinc in DMSO7Synthesis and Structural Characterization of Tris(isopropylbenzimidazol-2-ylthio)methyl Zinc Complexes, [Titm Pr i Benz ]ZnX: Modulation of Transannular Zn–C Interactions21A Series of 4- and 5-Coordinate Ni(II) Complexes: Synthesis, Characterization, Spectroscopic, and DFT Studies37Exploiting synergy between ligand design and counterion interactions to boost room temperature phosphorescence from Cu( i ) compounds40Reactivity of the carbodiphosphorane, (Ph 3 P) 2 C, towards main group metal alkyl compounds: coordination and cyclometalation13Thermodynamic targeting of electrocatalytic CO 2 reduction: advantages, limitations, and insights for catalyst design19Coordination of 1-methyl-1,3-dihydro-2H-benzimidazole-2-selone to zinc and cadmium: Monotonic and non-monotonic bond length variations for [H(sebenzimMe)]2MCl2 complexes (M = Zn, Cd, Hg)5Monomeric zinc(II) amide complexes supported by bidentate, benzannulated phenanthridine amido ligands17N-Heterocyclic Carbene Complexes of Copper, Nickel, and Cobalt468The effect of short alkane bridges in stability of bisbenzimidazole-2-ylidene silver(I) complexes: synthesis, crystal structure and antibacterial activity11Mononuclear, Dinuclear, and 1-D Chain Structural Variations in Zinc(4-fluoro-2-hydroxy-benzoic Acid)Bipyridine Complexes: Syntheses, Structures, and Luminescence Properties5Catalytic Conversion of Atmospheric CO2 into Organic Carbonates by Nickel(II) Complexes of Diazepane-Based N4 Ligands38Design, Synthesis, and Structure of Copper Dithione Complexes: Redox‐Dependent Charge Transfer14Copper-based redox shuttles supported by preorganized tetradentate ligands for dye-sensitized solar cells28Cu( i ) complexes obtained via spontaneous reduction of Cu( ii ) complexes supported by designed bidentate ligands: bioinspired Cu( i ) based catalysts for aromatic hydroxylation35Electrocatalytic hydrogen production by dinuclear cobalt( ii ) compounds containing redox-active diamidate ligands: a combined experimental and theoretical study22Tuning electronic structure through halide modulation of mesoionic carbene cobalt complexes13Nickel (II) and cobalt (II) complexes with bidentate nitrogen-sulfur donor pyrazole derivative ligands: Syntheses, characterization, X-ray structure, electrochemical studies, and antibacterial activity36Efficient removal of As(V) from simulated arsenic‐contaminated wastewater via a novel metal–organic framework material: Synthesis, structure, and response surface methodology14Synthesis and structural characterization of bis(2-pyridylthio)(p-tolylthio)methyl zinc complexes and the catalytic hydrosilylation of CO220Silver(I) and Copper(I) Complexes of Semi‐Bulky Nitrogen‐Confused C‐Scorpionates7Tetrahedral copper(I) complexes of novel N,N-bidentate ligands and photophysical properties28Siloxyaluminate and Siloxygallate Complexes as Models for Framework and Partially Hydrolyzed Framework Sites in Zeolites and Zeotypes3A Mononuclear and High-Spin Tetrahedral TiII Complex25Ni(0)-promoted activation of C sp2 –H and C sp2 –O bonds12Selective propargylic C(sp 3 )–H activation of methyl-substituted alkynes versus [2 + 2] cycloaddition at a titanium imido template7The Coordination Chemistry of Low-Valent Nickel, Palladium, and Platinum1N-Heterocyclic Carbene Complexes of Nickel, Palladium, and Iridium Derived from Nitron: Synthesis, Structures, and Catalytic Properties27New mix-ligand copper(i) and copper(ii) pyrazolate complexes with 2,2′-bipyridine13High‐spin square planar iron(II) alkali metal siloxide complexes – influence of the alkali metal and reactivity towards O2 and NO7Mimicking of the histidine brace structural motif in molecular copper(I) compounds4Gold-to-Boron Aryl Transfer from a T-Shaped Phosphine–Borane Gold(I) Complex8C−C Cross‐Couplings from a Cyclometalated Au(III) CN Complex: Mechanistic Insights and Synthetic Developments11A mixed-valent high spin (μ-hydroxo)dicobalt(II/III) complex and its end-on type dioxygen adduct: synthesis, geometric and electronic structure studies4Platinum( ii ) complexes of benzannulated N ∧ N −∧ O-amido ligands: bright orange phosphors with long-lived excited states12Mononuclear Copper(I) 3-(2-pyridyl)pyrazole Complexes: The Crucial Role of Phosphine on Photoluminescence18Two-dimensional zinc(II) and copper(I) coordination polymers for photoluminescence8Binding of carbon monoxide at a single nickel center and its oxidative reactivity toward CO 2 and O 26Heteroleptic copper( i ) charge-transfer chromophores with panchromatic absorption23Mononuclear copper( ii ) Schiff base complexes as effective models for phenoxazinone synthase32N-Heterocyclic Carbene Complexes of Nickel2Reaction of a bis(pentafulvene)titanium complex with an N-heterocyclic olefin: C–H-activation leads to resonance between a titanium vinyl and titanium alkylidene complex10Iron(II) Mediated Deazotation of Benzyl Azide: Trapping and Subsequent Transformations of the Benzaldimine Fragment8Zn Metal–Organic Framework with High Stability and Sorption Selectivity for CO236Heteroleptic nickel complexes bearing O‐methyldithiophosphate and aminodiphosphine monosulfide ligands as robust molecular electrocatalysts for hydrogen evolution5Zinc-based cyclens containing pyridine and cross-bridges: X-ray and DFT structures, Lewis acidity, gas-phase acidity, and pKa values1The development of an unexpected Cu(I)‐pyrazolo pyrimidine‐based complex: Synthesis, spectroscopic characterizations, and biological activity8Main group catalysis for H 2 purification based on liquid organic hydrogen carriers44The anticancer impacts of N, S donor pyrazole based ligand and its Co(III) and Cu(II) complexes on breast cancer cells2Are Zn( ii ) pincer complexes efficient apoptosis inducers? a deep insight into their activity against A549 lung cancer cells13The supramolecular frameworks and electrocatalytic properties of two new structurally diverse tertiary phosphane-appended nickel( ii ) and copper( i ) thiosquarates32A Contiguous Tricyclic [P6]2– Framework Spanning Across Two Vanadium(III) Centers1Highly Distorted Bismuth–Nickel(II) Complex6Remote Back Strain: A Strategy for Modulating the Reactivity of Triarylboranes12Synthesis, crystal structure and protein binding studies of a binuclear copper(I) complex with triphenylphosphine based dithiocarbazate8Deciphering the Mechanism of MRSA Targeting Copper(II) Complexes of NN2 Pincer-Type Ligands11Effect of Co/SiO2 Single-Site Heterogeneity on Small Alkane Dehydrogenation Kinetics6A phosphine-free molecularly-defined Ni( ii ) complex in catalytic hydrogenation of CO 24New heteroleptic bis-(diphenylphosphino)ethane appended dialkyldithiophosphate cobalt( iii ) cations: apt electrocatalysts for the heterogeneous oxygen evolution reaction and homogeneous hydrogen evolution reaction26NHC-ligated nickel( ii ) cyanoborate complexes and salts4Reactivity of low-valent nickel carbonyl species supported by acridane based PNP ligands towards iodoalkanes4Geometry indices for four- and five-coordinate metal complexes: a concise review34Ni(II), Pd(II) and Cu(II) coordination complexes of a π-extended dianionic N^N−^N−^N ligand: Synthesis, structures and electronic absorption spectroscopy2Selective Manipulation of Well‐Defined Trinuclear Pd(II)‐Complexes3Air-Stable Dinuclear Complexes of Four-Coordinate ZnII and NiII Ions with a Radical Bridge: A Detailed Look at Redox Activity and Antiferromagnetic Coupling8C−H Bond Activation Facilitated by Nickel(II) Complexes Having Mighty Claws7A nickel metalloradical bearing a phenalenyl-based tridentate ligand3Synthesis and structural characterization of 2,2’-bipyridine zinc formate: Analysis of formate bonding and hydrosilylation of CO2 and carbonyl compounds1Site‐Selective Ligand Functionalization Reverses Hypsochromic Luminescence Shifts in Platinum(II) Complexes of Benzannulated NCN ‐Coordinating Ligands5New positional isomeric homoleptic Ni(II) dithiolate anions as molecular homogeneous electrocatalysts for hydrogen evolution reaction7Copper( ii ) complex with a redox-noninnocent Schiff base bearing a tetraphenyldisiloxane unit: synthesis, structure and catalytic oxidation of cyclohexane4Revisiting the structure and properties of mid-valent monopentamethylcyclopentadienylchromium complexes1Monodentate σ-Accepting Boron-Based Ligands Bearing Square-Planar Ni(0) Centers10Electronic structure of mononuclear and radical-bridged dinuclear cobalt(II) single-molecule magnets18Metal-α-Helix Peptide Frameworks20Synthesis of Heterodinuclear Cobalt(III)/Silver(I) Complexes and Their Catalytic Exploration for Ring-Opening Copolymerization of Carbon Dioxide with Terminal Epoxides4Active Sites in the Dealuminated Beta Zeolite-Supported Cobalt Catalyst for Non-Oxidative Ethane Dehydrogenation17Copper-Based Redox Shuttles Supported by Pentadentate Ligands for Dye-Sensitized Solar Cells with Enhanced Efficiencies under Low-Light Conditions0Two dinuclear cobalt-hydroxo complexes derived from Salen-ligated cobalt precursors: Crystal structures, spectroscopic characterizations, DFT calculations and property studies1Synthesis and anticancer activity of six tricyclohexyltin cinnamate complexes5In Pursuit of Low Energy Phosphorescence: Late Metal Coordination Complexes of the Planar, π‐extended Bipyridyl Ligand 6,6′,7,7′‐Biphenanthridine2The structural parameter of spin states of C 1 -symmetric four-coordinate cobalt complexes: D 46Gold( iii ) complexes of 2- tert -butyl-1,10-phenanthroline and of N -(8-quinolinyl)amides: syntheses and structures0Unveiling the acid properties of metallosilicate nanospheres: a combined experimental and computational study0Inter‐/Intramolecular π ‐Stacking in a Benzannulated NCN‐Coordinated Pd(II) Monomer and Dimer Pair: Synthesis, Structure, and Photophysics0Group 10 Metal Complexes Featuring Rigid Phenylene-Bridged NHC/Pyridyl Ligands: Controlling Coordination Modes, Electrochemical Properties, and CO 2 Reduction Catalysis1NHC based Pd-PEPPSI complexes: synthesis, computational studies and application for Suzuki and direct arylation reactions1Synthesis and cytotoxic activity of S-alkylated Isothiosemicarbazone Ni(II) complexes with methyl-substituted pyridine co-ligands: Experimental and computational insights0Synthesis and Structural Characterization of Bis (2-pyridylthio)methyl Cadmium Compounds: Access to a Six-Coordinate Cadmium Dialkyl Complex0Two routes, one framework: Tuning acidity and catalytic activity of Zr(IV) and Hf(IV)-doped hollow silica nanospheres0Reactivity of [Pt2(PP)2(μ-Cl)2][BArF24]2 (PP = 1,1ʹ-bis(phosphino)ferrocene; BArF24 = tetrakis(3,5-bis(trifluoromethyl)phenyl)borate)) compounds with monodentate phosphines0Experimental and Quantum-Chemical Characterization of an Imidazolidin-2-Ylidene-Based Pd-PEPPSI Complex0Synthesis, structural characterization, and acaricidal activity of novel cyclohexyltin carboxylate complexes0

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  1. Introducing a pyrazole/imidazole based hybrid cyclophane: a hydrogen bond sensor and binucleating ligand precursor

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  4. Probing the Limits of Tetraazamacrocycle‐Glyoxal Condensates as Bidentate Ligands for Cu2+

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  5. Supramolecular Assembly of Metal‐Organic Tubes Constructed from the Ditopic Heteroscorpionate Ligand (4‐NH2C6H4)CHpz2 (pz = Pyrazol‐1‐yl) and Silver(I)

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  35. Monomeric zinc(II) amide complexes supported by bidentate, benzannulated phenanthridine amido ligands

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  38. Mononuclear, Dinuclear, and 1-D Chain Structural Variations in Zinc(4-fluoro-2-hydroxy-benzoic Acid)Bipyridine Complexes: Syntheses, Structures, and Luminescence Properties

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  39. Catalytic Conversion of Atmospheric CO2 into Organic Carbonates by Nickel(II) Complexes of Diazepane-Based N4 Ligands

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  40. Design, Synthesis, and Structure of Copper Dithione Complexes: Redox‐Dependent Charge Transfer

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  44. Tuning electronic structure through halide modulation of mesoionic carbene cobalt complexes

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