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RESEARCH PAPER · Journal of the American Chemical Society · 2009

Phase Transformation of Biphasic Cu2S−CuInS2 to Monophasic CuInS2 Nanorods

Stephen T. Connor, Ching-Mei Hsu, Benjamin D. Weil, Shaul Aloni, Yi Ping Cui

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Phase Transformation of Biphasic Cu2S−CuInS2 to Monophasic CuInS2 NanorodsOriginalPhase-Selective Synthesis of CuInS2 Nanocrystals137Synthesis, Characterization, and Growth Mechanism of n-Type CuInS2 Colloidal Particles86Growth Kinetics of Monodisperse Cu−In−S Nanocrystals Using a Dialkyl Disulfide Sulfur Source126Electronic Structure and E[sub 1] Excitons of CuInS[sub 2] Energy-Related Crystals Studied by Temperature-Dependent Thermoreflectance Spectroscopy11Highly conducting two-dimensional copper(i) 4-hydroxythiophenolate network76Magnetically-induced synthesis of highly-crystalline ternary chalcopyrite nanocrystals under ambient conditions9Ordered arrays of shape tunable CuInS2 nanostructures, from nanotubes to nano test tubes and nanowires38Shape controlled synthesis of tadpole-like and heliotrope seed-like AgInS2 nanocrystals48Polarized-thermoreflectance study of the band-edge transitions in Cu(Al_05In_05)S_2 solar-energy related crystal9Synthesis of Metastable Wurtzite CuInSe 2 Nanocrystals177Synthesis and characterization of phase-purity Cu9BiS6 nanoplates9Synthesis of n-type CuInS2 Particles Using N-methylimidazole, Characterization and Growth Mechanism63Facile synthesis of nanocrystalline wurtzite Cu–In–S by amine-assisted decomposition of precursors26Noninjection Gram-Scale Synthesis of Monodisperse Pyramidal CuInS2 Nanocrystals and Their Size-Dependent Properties421Hybrid nanoscale inorganic cages133Synthesis and Shape Control of CuInS2 Nanoparticles294Synthesis of Au−Cu2S Core−Shell Nanocrystals and Their Photocatalytic and Electrocatalytic Activity95Controllable Growth of Semiconductor Heterostructures Mediated by Bifunctional Ag2S Nanocrystals as Catalyst or Source-Host182Charge transfer in blends of P3HT and colloidally prepared CuInS2 nanocrystals17Controlled synthesis of wurtzite CuInS2 nanocrystals and their side-by-side nanorod assemblies107Fabrication of single crystal CuGaS2 nanorods by X-ray irradiation27Facile one-pot synthesis of copper sulfide–metal chalcogenide anisotropic heteronanostructures in a noncoordinating solvent39Facile thermolysis synthesis of CuInS2 nanocrystals with tunable anisotropic shape and structure79Temperature Dependent Crystal-Field Splitting and Band-Edge Characteristic in Cu(AlxIn1-x)S2 (0 ≤ x ≤ 1) Series Solar Energy Materials8Single crystal growth and characterization of copper aluminum indium disulfide chalcopyrites10Growth of CuI buffer layer prepared by spraying method23Microstructure and optical properties of sprayed γ‐CuI thin films for CuInS 2 solar cells9From Ultrathin Two-Dimensional Djurleite Nanosheets to One-Dimensional Nanorods Comprised of Djurleite Nanoplates: Synthesis, Characterization, and Formation Mechanism24Facile Synthesis of ZnS−CuInS2-Alloyed Nanocrystals for a Color-Tunable Fluorchrome and Photocatalyst250CuInSe2 nano-crystallite reaction kinetics using solid state reaction from Cu2Se and In2Se3 powders17Optical Characterization of Electronic Structure of CuInS2 and CuAlS2 Chalcopyrite Crystals1Synthesis of Cu2–xSe Nanocrystals by Tuning the Reactivity of Se28Investigations of solvents and various sulfur sources influence on the shape-controlled synthesis of CuInS2 nanocrystals44Synthesis of Shape-Controlled Monodisperse Wurtzite CuIn x Ga 1– x S 2 Semiconductor Nanocrystals with Tunable Band Gap192Ionic compounds lamination reaction and characteristics of photosensitive copper indium sulfide on titania nanotube arrays9Sphere-like CuGaS2 nanoparticles synthesized by a simple biomolecule-assisted solvothermal route38Fabrication and characterization of indium sulfide thin films deposited on SAMs modified substrates surfaces by chemical bath deposition20One-pot route for preparation of monodisperse CuInS2 nanocrystals11Growth of CuInSe2 and In2Se3/CuInSe2 Nano-Heterostructures through Solid State Reactions44Synthesis of hexagonal structured wurtzite and chalcopyrite CuInS2 via a simple solution route36Photochemical deposition of Ag nanocrystals on hierarchical ZnO microspheres and their enhanced gas-sensing properties84Study of sulphidation of Cu–In nanoparticle precursor films with an air-stable process0New strategy to the controllable synthesis of CuInS2 hollow nanospheres and their applications in lithium ion batteries25Synthesis and characterization of flower-like CuIn1−xGaxS2 (x=0.3) microspheres3Crystal phase-controlled synthesis of Cu2FeSnS4 nanocrystals with a band gap of around 1.5 eV134Fabrication of single-crystalline CuInS2 nanowires array via a diethylenetriamine-thermal route21Inorganic ligand mediated synthesis of CuInS2 nanocrystals with tunable properties16iso-Propylthiobiuret-copper and indium complexes as novel precursors for colloidal synthesis of CuInS2 nanoparticles27New organometallic single-source precursors for CuGaS2 – polytypism in gallite nanocrystals obtained by thermolysis30Synthesis of band-gap tunable Cu–In–S ternary nanocrystals in aqueous solution21Thin-Film Technology in Intermediate Band Solar Cells: Advanced Concepts for Chalcopyrite Solar Cells3Colloidal Synthesis of Wurtzite Cu 2 ZnSnS 4 Nanorods and Their Perpendicular Assembly403Colloidal Nanocrystals of Wurtzite‐Type Cu2ZnSnS4: Facile Noninjection Synthesis and Formation Mechanism144Evolution Pathway of CIGSe Nanocrystals for Solar Cell Applications61Alkylthiol-Enabled Se Powder Dissolution in Oleylamine at Room Temperature for the Phosphine-Free Synthesis of Copper-Based Quaternary Selenide Nanocrystals230Surface sensing behavior and band edge properties of AgAlS2: Experimental observations in optical, chemical, and thermoreflectance spectroscopy15Solvothermal Synthesis of Zincblende and Wurtzite CuInS2 Nanocrystals and Their Photovoltaic Application128One‐Pot Controlled Synthesis of Hexagonal‐Prismatic Cu1.94S‐ZnS, Cu1.94S‐ZnS‐Cu1.94S, and Cu1.94S‐ZnS‐Cu1.94S‐ZnS‐Cu1.94S Heteronanostructures72One‐Pot Controlled Synthesis of Hexagonal‐Prismatic Cu1.94S‐ZnS, Cu1.94S‐ZnS‐Cu1.94S, and Cu1.94S‐ZnS‐Cu1.94S‐ZnS‐Cu1.94S Heteronanostructures5Alloyed (ZnS)x(CuInS2)1−x Semiconductor Nanorods: Synthesis, Bandgap Tuning and Photocatalytic Properties68Phase control and its mechanism of CuInS2 nanoparticles38Solvothermal synthesis of nanostructured CuInS2 thin films on FTO substrates and their photoelectrochemical properties47Synthesis of bullet-like wurtzite CuInS2 nanocrystals under atmospheric conditions23Facile synthesis of ZnS–CdIn2S4-alloyed nanocrystals with tunable band gap and its photocatalytic activity8Facile synthesis of wurtzite copper–zinc–tin sulfidenanocrystals from plasmonic djurleite nuclei58Synthesis, photoconductivity and self-assembly of wurtzite phase Cu 2 Cd x Zn 1−x SnS 4 nanorods39Structural and Band-Edge Properties of Cu(AlxIn1-X)S2 (0≤x≤1) Series Chalcopyrite Semiconductors3Wurtzite CuInS2 and CuInxGa1−xS2 nanoribbons: synthesis, optical and photoelectrical properties51Colloidal synthesis and optical properties of metastable wurtzite I3-III-IV-VI5 (Cu3InSnS5) nanocrystals13Controllable synthesis of metal selenide heterostructures mediated by Ag2Se nanocrystals acting as catalysts27Controlled synthesis of CuInS2, Cu2SnS3 and Cu2ZnSnS4 nano-structures: insight into the universal phase-selectivity mechanism134Fabrication and Characterization of Thin Film Solar Cell Made from CuIn 0.75 Ga 0.25 S 2 Wurtzite Nanoparticles5Facile synthesis and characterization of CuInS2 nanocrystals with different structures and shapes35One dimensional CuInS2–ZnS heterostructured nanomaterials as low-cost and high-performance counter electrodes of dye-sensitized solar cells171Precursor driven one pot synthesis of wurtzite and chalcopyrite CuFeS243Solution-based synthesis of wurtzite Cu2ZnSnS4 nanoleaves introduced by α-Cu2S nanocrystals as a catalyst22Synthesis of wurtzite CuInS2 nanowires by Ag2S-catalyzed growth44Ternary and quaternary metal chalcogenide nanocrystals: synthesis, properties and applications633Wet-Chemical Synthesis and Optical Property of ZnSe Nanowires by Ag2Se-Catalyzed Growth Mechanism9Wurtzite CuInS2: solution based one pot direct synthesis and its doping studies with non-magnetic Ga3+ and magnetic Fe3+ ions32Behaviors of Fe, Zn, and Ga Substitution in CuInS2 Nanoparticles Probed with Anomalous X-ray Diffraction21Systematic Study into the Synthesis and Shape Development in Colloidal CuInxGa1–xS2 Nanocrystals55Colloidal synthesis of wurtzite Cu2CoSnS4 nanocrystals and the photoresponse of spray-deposited thin films56Optical properties of wide-band-gap chalcopyrite CuAl(Se_05S_05)_2 evaluated by thermoreflectance spectroscopy5Phase-controllable synthesis of CuxS nanocrystals by an ambient pressure tetraethylene glycol solution process7Sacrificial Template Synthesis and Photothermal Conversion Enhancements of Hierarchical and Hollow CuInS2 Microspheres43Colloidal Synthesis of Ternary AgFeS2 Nanocrystals and Their Transformation to Ag2S‐Fe7S8 Heterodimers26Hydrothermal fabrication of chalcopyrite-type CuInS2 film and their optical properties6Highly reactive, flexible yet green Se precursor for metal selenide nanocrystals: Se-octadecene suspension (Se-SUS)139CuIn x Ga1– x S2 Nanocrystals with Tunable Composition and Band Gap Synthesized via a Phosphine-Free and Scalable Procedure67Spinel Indium Sulfide Precursor for the Phase-Selective Synthesis of Cu–In–S Nanocrystals with Zinc-Blende, Wurtzite, and Spinel Structures71Near-Infrared Absorbing Cu12Sb4S13 and Cu3SbS4 Nanocrystals: Synthesis, Characterization, and Photoelectrochemistry183Solution–Solid–Solid Mechanism: Superionic Conductors Catalyze Nanowire Growth90Fabrication of hollow-sphere films of wurtzite CuInS2 on copper substrate9A generalized strategy for controlled synthesis of ternary metal sulfide nanocrystals49Solvothermal synthesis of CuInS2 powders and CuInS2 thin films for solar cell application11Colloidal Synthesis of CuInS2and CuInSe2Nanocrystals for Photovoltaic Applications2R aman scattering in orthorhombic Cu I n S 2 nanocrystals26Synthesis and Application of Colloidal CuInS 2 Semiconductor Nanocrystals461Formation of AgGaS2 nano-pyramids from Ag2S nanospheres through intermediate Ag2S–AgGaS2 heterostructures and AgGaS2 sensitized Mn2+ emission42Solution-phase catalytic synthesis, characterization and growth kinetics of Ag 2 S–CdS matchstick-like heteronanostructures29Fabrication of a CuInS 2 photoelectrode using a single-step electrodeposition with controlled calcination atmosphere23Colloidal semiconductor nanocrystals: controlled synthesis and surface chemistry in organic media173Controllable growth of Ag 2 S–CdS heteronanostructures21One-step synthesis of near-infrared emitting and size tunable CuInS 2 semiconductor nanocrystals by adjusting kinetic variables25Synthesis and formation mechanism of CuInS 2 nanocrystals with a tunable phase33Synthesis of metastable wurtzite CuInS2 nanocrystals and films from aqueous solution13Synthesis of wurtzite–zincblende Cu2ZnSnS4 and Cu2ZnSnSe4 nanocrystals: insight into the structural selection of quaternary and ternary compounds influenced by binary nuclei58Synthesis and investigation of optical properties of TOPO-capped CuInS2 semiconductor nanocrystal in the presence of different solvent13One-Pot Controlled Synthesis of Spongelike CuInS2 Microspheres for Efficient Counter Electrode with Graphene Assistance in Dye-Sensitized Solar Cells53Ag 2 S – CoS 2 hetero-nanostructures: One-pot colloidal synthesis and improved magnetic properties2Structure and morphology evolution in mechanochemical processed CuInS2 powder15Mild solution-based method for synthesizing wurtzite CuInS2 nanoplates at low temperature11Selective synthesis of cubic and hexagonal phase of CuInS 2 nanocrystals by microwave irradiation17Complete Colloidal Synthesis of Cu2SnSe3 Nanocrystals with Crystal Phase and Shape Control85Synthesis of copper sulphide-based hybrid nanostructures and their application in shape control of colloidal semiconductor nanocrystals44Efficient Thermolysis Route to Monodisperse Cu2ZnSnS4 Nanocrystals with Controlled Shape and Structure66Optical behavior and structural property of CuAlS2 and AgAlS2 wide-bandgap chalcopyrites13Copper‐Based Ternary and Quaternary Semiconductor Nanoplates: Templated Synthesis, Characterization, and Photoelectrochemical Properties137Copper‐Based Ternary and Quaternary Semiconductor Nanoplates: Templated Synthesis, Characterization, and Photoelectrochemical Properties33Controllable Synthesis of Wurtzite Cu2ZnSnS4 Nanocrystals by Hot‐Injection Approach and Growth Mechanism Studies16Colloidal synthesis of CuGaS x Se 2 − x nanoribbons mediated by Cu 1.75 (SSe) nanocrystals as catalysts10Structural and Optical Study of Ga 3+ Substitution in CuInS 2 Nanoparticles Synthesized by a One-Pot Facile Method32Morphology-controlled growth of special nanostructure CuInS2 thin films on an FTO substrate and their application in thin film solar cells18Characteristics of Cu2ZnSnS4Thin Films Fabricated by Sulfurization of Two Stacked Metallic Layers5Role of Copper Sulfide Seeds in the Growth Process of CuInS2 Nanorods and Networks60Growth of nanosheet array and nanosheet microsphere CuInS2 thin films on transparent conducting substrates3Interlaced crystals having a perfect Bravais lattice and complex chemical order revealed by real-space crystallography40The synthesis of hollow CuInS2 microspheres with hierarchical structures4Structural and optical properties of Fe and Zn substituted CuInS 2 nanoparticles synthesized by a one-pot facile method20Nanocluster seed-mediated synthesis of CuInS 2 quantum dots, nanodisks, nanorods, and doped Zn-CuInGaS 2 quantum dots53Microwave heating synthesis and formation mechanism of chalcopyrite structured CuInS2 nanorods in deep eutectic solvent20Pulsed laser deposition of single-crystalline Cu7In3/CuIn0.8Ga0.2Se2 core/shell nanowires3Synthesis of CZTSSe Thin Films from Nanocrystal Inks12AACVD of Cu 2−x S, In 2 S 3 and CuInS 2 thin films from [Cu( i Bu 2 PS 2 )(PPh 3 ) 2 ] and [In( i Bu 2 PS 2 ) 3 ] as single source precursors14Alloyed CuInS 2 –ZnS nanorods: synthesis, structure and optical properties38Colloidal nanocrystals of orthorhombic Cu 2 ZnGeS 4 : phase-controlled synthesis, formation mechanism and photocatalytic behavior46Complete study of the composition and shape evolution in the synthesis of Cu 2 ZnSnS 4 (CZTS) semiconductor nanocrystals41One-pot synthesis of CuInS 2 nanocrystals using different anions to engineer their morphology and crystal phase38Phase dependent visible to near-infrared photoluminescence of CuInS 2 nanocrystals35Synthesis of CuInS 2 nanocrystals from a molecular complex – characterization of the orthorhombic domain structure12Synthesis of CuInS2-ZnS Alloyed Nanorods and Hybrid Nanostructures1The role of interparticle heterogeneities in the selenization pathway of Cu–Zn–Sn–S nanoparticle thin films: a real-time study21Surface Sensing and Optical Behavior of Al-Based Silver Chalcopyrites0Polarized optical sensing and band-edge transitions in Ag(In0.5Al0.5)S21Phase-controlled synthesis of Cu2ZnSnS4 powders via the microwave-assisted solvothermal route20The Heat-Up Synthesis of Colloidal Nanocrystals414The phase transformation of CuInS2 from chalcopyrite to wurtzite80Morphology-Controlled Synthesis of Au/Cu2FeSnS4 Core–Shell Nanostructures for Plasmon-Enhanced Photocatalytic Hydrogen Generation653D hierarchical FeSe2 microspheres: Controlled synthesis and applications in dye-sensitized solar cells151

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  1. Phase-Selective Synthesis of CuInS2 Nanocrystals

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  2. Synthesis, Characterization, and Growth Mechanism of n-Type CuInS2 Colloidal Particles

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  3. Growth Kinetics of Monodisperse Cu−In−S Nanocrystals Using a Dialkyl Disulfide Sulfur Source

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  4. Electronic Structure and E[sub 1] Excitons of CuInS[sub 2] Energy-Related Crystals Studied by Temperature-Dependent Thermoreflectance Spectroscopy

    Journal of The Electrochemical Society · 2009-12-31

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  5. Highly conducting two-dimensional copper(i) 4-hydroxythiophenolate network

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  6. Magnetically-induced synthesis of highly-crystalline ternary chalcopyrite nanocrystals under ambient conditions

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  7. Ordered arrays of shape tunable CuInS2 nanostructures, from nanotubes to nano test tubes and nanowires

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  8. Shape controlled synthesis of tadpole-like and heliotrope seed-like AgInS2 nanocrystals

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  9. Polarized-thermoreflectance study of the band-edge transitions in Cu(Al_05In_05)S_2 solar-energy related crystal

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  10. Synthesis of Metastable Wurtzite CuInSe 2 Nanocrystals

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  11. Synthesis and characterization of phase-purity Cu9BiS6 nanoplates

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  12. Synthesis of n-type CuInS2 Particles Using N-methylimidazole, Characterization and Growth Mechanism

    Chemistry of Materials · 2010-05-17

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  13. Facile synthesis of nanocrystalline wurtzite Cu–In–S by amine-assisted decomposition of precursors

    Journal of Solid State Chemistry · 2010-06-20

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  14. Noninjection Gram-Scale Synthesis of Monodisperse Pyramidal CuInS2 Nanocrystals and Their Size-Dependent Properties

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  15. Hybrid nanoscale inorganic cages

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  16. Synthesis and Shape Control of CuInS2 Nanoparticles

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  17. Synthesis of Au−Cu2S Core−Shell Nanocrystals and Their Photocatalytic and Electrocatalytic Activity

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  18. Controllable Growth of Semiconductor Heterostructures Mediated by Bifunctional Ag2S Nanocrystals as Catalyst or Source-Host

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  19. Charge transfer in blends of P3HT and colloidally prepared CuInS2 nanocrystals

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  20. Controlled synthesis of wurtzite CuInS2 nanocrystals and their side-by-side nanorod assemblies

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  21. Fabrication of single crystal CuGaS2 nanorods by X-ray irradiation

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  22. Facile one-pot synthesis of copper sulfide–metal chalcogenide anisotropic heteronanostructures in a noncoordinating solvent

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  23. Facile thermolysis synthesis of CuInS2 nanocrystals with tunable anisotropic shape and structure

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  24. Temperature Dependent Crystal-Field Splitting and Band-Edge Characteristic in Cu(AlxIn1-x)S2 (0 ≤ x ≤ 1) Series Solar Energy Materials

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  25. Single crystal growth and characterization of copper aluminum indium disulfide chalcopyrites

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  26. Growth of CuI buffer layer prepared by spraying method

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  27. Microstructure and optical properties of sprayed γ‐CuI thin films for CuInS 2 solar cells

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  28. From Ultrathin Two-Dimensional Djurleite Nanosheets to One-Dimensional Nanorods Comprised of Djurleite Nanoplates: Synthesis, Characterization, and Formation Mechanism

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  29. Facile Synthesis of ZnS−CuInS2-Alloyed Nanocrystals for a Color-Tunable Fluorchrome and Photocatalyst

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  30. CuInSe2 nano-crystallite reaction kinetics using solid state reaction from Cu2Se and In2Se3 powders

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  33. Investigations of solvents and various sulfur sources influence on the shape-controlled synthesis of CuInS2 nanocrystals

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  34. Synthesis of Shape-Controlled Monodisperse Wurtzite CuIn x Ga 1– x S 2 Semiconductor Nanocrystals with Tunable Band Gap

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  35. Ionic compounds lamination reaction and characteristics of photosensitive copper indium sulfide on titania nanotube arrays

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  36. Sphere-like CuGaS2 nanoparticles synthesized by a simple biomolecule-assisted solvothermal route

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  37. Fabrication and characterization of indium sulfide thin films deposited on SAMs modified substrates surfaces by chemical bath deposition

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  38. One-pot route for preparation of monodisperse CuInS2 nanocrystals

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  39. Growth of CuInSe2 and In2Se3/CuInSe2 Nano-Heterostructures through Solid State Reactions

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  40. Synthesis of hexagonal structured wurtzite and chalcopyrite CuInS2 via a simple solution route

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  41. Photochemical deposition of Ag nanocrystals on hierarchical ZnO microspheres and their enhanced gas-sensing properties

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  42. Study of sulphidation of Cu–In nanoparticle precursor films with an air-stable process

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  43. New strategy to the controllable synthesis of CuInS2 hollow nanospheres and their applications in lithium ion batteries

    Journal of Solid State Chemistry · 2011-12-08

    Weixin Zhang, Hui Dan Zeng, Zeheng Yang, Qiang Wang

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  44. Synthesis and characterization of flower-like CuIn1−xGaxS2 (x=0.3) microspheres

    Materials Research Bulletin · 2011-12-08

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  45. Crystal phase-controlled synthesis of Cu2FeSnS4 nanocrystals with a band gap of around 1.5 eV

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  46. Fabrication of single-crystalline CuInS2 nanowires array via a diethylenetriamine-thermal route

    CrystEngComm · 2012-01-01

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  47. Inorganic ligand mediated synthesis of CuInS2 nanocrystals with tunable properties

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    Jingjing He, Wenhui Zhou, Jie Guo, Mei Li, Sixin Wu

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  48. iso-Propylthiobiuret-copper and indium complexes as novel precursors for colloidal synthesis of CuInS2 nanoparticles

    Journal of Materials Chemistry · 2012-01-01

    Ahmed Lutfi Abdelhady, Mohammad Azad Malik, Paul O’Brien

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  49. New organometallic single-source precursors for CuGaS2 – polytypism in gallite nanocrystals obtained by thermolysis

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