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RESEARCH PAPER · Journal of Alloys and Compounds · 2013

Synthesis, structure, physicochemical characterization and electronic structure of thio-lithium super ionic conductors, Li4GeS4 and Li4SnS4

Joseph H. MacNeil, Danielle M. Massi, Jian‐Han Zhang, Kimberly A. Rosmus, Carl D. Brunetta, Taylor A. Gentile, Jennifer A. Aitken

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Synthesis, structure, physicochemical characterization and electronic structure of thio-lithium super ionic conductors, Li4GeS4 and Li4SnS4OriginalThree new chalcohalides, Ba4Ge2PbS8Br2, Ba4Ge2PbSe8Br2 and Ba4Ge2SnS8Br2: Syntheses, crystal structures, band gaps, and electronic structures4Synthesis of single phase cubic Al-substituted Li7La3Zr2O12 by solid state lithiation of mixed hydroxides48Synthesis and structure of novel lithium-ion conductor Li7Ge3PS1260Cubic Rocksalt Li2SnS3 and a Solid Solution with Li3NbS4 Prepared by Mechanochemical Synthesis15Room‐Temperature Synthesis of Three Compounds Featuring the [Ge4S10]4– Anion from a Water‐Soluble Thiogermanate Precursor7Cathode materials and sulfide solid electrolytes for lithium battery0Appearance of Lithium-Ion Conduction in a La–Li–Co–O Band Insulator: Possible Route to Oxide Electrolyte12Mechanochemical Synthesis and Characterization of Metastable Hexagonal Li4SnS4 Solid Electrolyte102Lithium Transport in Li4.4 M 0.4 M ′0.6S4 (M = Al3+, Ga3+, and M ′ = Ge4+, Sn4+): Combined Crystallographic, Conductivity, Solid State NMR, and Computational Studies39Influence of the Lithium Substructure on the Diffusion Pathways and Transport Properties of the Thio-LISICON Li 4 Ge 1– x Sn x S 456Li4-Sb Sn1-S4 solid solutions for air-stable solid electrolytes99Phase Stability and Electronic Structure of Tin Sulfide Compounds for Li-ion Batteries4Materials design of ionic conductors for solid state batteries238All-solid-state lithium batteries enabled by sulfide electrolytes: from fundamental research to practical engineering design489Impact of hydration on ion transport in Li 2 Sn 2 S 5 · x H 2 O22Ternary alkali ion thiogallates, A 5 GaS 4 (A = Li and Na), with isolated tetrahedral building units and their ionic conductivities20Two-Dimensional Substitution: Toward a Better Understanding of the Structure–Transport Correlations in the Li-Superionic Thio-LISICONs26Tracking Ions the Direct Way: Long-Range Li+ Dynamics in the Thio-LISICON Family Li4MCh4 (M = Sn, Ge; Ch = S, Se) as Probed by 7Li NMR Relaxometry and 7Li Spin-Alignment Echo NMR43Insights into the Electrochemical Stability and Lithium Conductivity of Li4MS4 (M = Si, Ge, and Sn)12Progress in thermal stability of all‐solid‐state‐Li‐ion‐batteries286Lithium phosphosulfide electrolytes for solid-state batteries: Part I27Mechanical Properties of Solid State Li-Ion Batteries0Thermal Stability between Sulfide Solid Electrolytes and Oxide Cathode122Determination of Gibbs Free Energy in the Compound Formation of Li-P and Li-Fe-O by Pymatgen2Current Status and Future Directions in Environmental Stability of Sulfide Solid-State Electrolytes for All-Solid-State Batteries100Enhanced Li-Ion Conductivity and Air Stability of Sb-Substituted Li4GeS4 toward All-Solid-State Li-Ion Batteries31EwaldSolidSolution: A High-Throughput Application to Quickly Sample Stable Site Arrangements for Ionic Solid Solutions11Li-Ion Conductivity of Single-Step Synthesized Glassy-Ceramic Li10GeP2S12 and Post-heated Highly Crystalline Li10GeP2S1217Matching strategy between sulfide solid electrolyte and various anodes: electrolyte modification, interface engineering and electrode structure design25An ab initio study on the elasticity and optical features of semiconductor lithium-based germanate chalcogenides (Li8GeS6 and Li8GeSe6)1From non-innocent ionic liquids to reactive agents in the synthesis of chalcogenido metalate compounds1Dimensional Reduction Guides Electronic Structure Evolution in the A n Cu 4– n SnS 4 Semiconductor Series9Structure and Transport Properties in the Pseudobinary Phase System Li4SiS4–Li4SnS46Establishement of generalized empirical force-fields for sulfide glasses and crystals used as superionic electrolytes in all-solid-state batteries0Mechanistic Understanding of Thermal Stability and Safety in Lithium Metal Batteries63Investigation of the Crystal‐Structure‐Dependent Moisture Stability of the Sulfide Solid Electrolyte Li 4 SnS 41Bridging chemistry and composition-space exploration: Particle swarm optimization of multicomponent glassy sulfide electrolytes0Anion Engineering of Sulfide Solid Electrolytes: From Fundamentals to High‐Performance All‐Solid‐State Batteries0Lithium Makes the Difference─Evolution of Lithium Vacancy Disorder during Temperature-Induced Phase Transitions of the Li-Ion Conductor Li4SnS40

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  1. Three new chalcohalides, Ba4Ge2PbS8Br2, Ba4Ge2PbSe8Br2 and Ba4Ge2SnS8Br2: Syntheses, crystal structures, band gaps, and electronic structures

    Journal of Alloys and Compounds · 2014-05-22

    Zuohong Lin, Kai Feng, Heng Tu, Lei Kang, Zheshuai Lin, Jiyong Yao, Yicheng Wu

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  2. Synthesis of single phase cubic Al-substituted Li7La3Zr2O12 by solid state lithiation of mixed hydroxides

    Journal of Alloys and Compounds · 2015-05-05

    Frederieke Langer, Jens Glenneberg, Ingo Bardenhagen, Róbert Kun

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  3. Synthesis and structure of novel lithium-ion conductor Li7Ge3PS12

    Journal of Solid State Chemistry · 2016-12-06

    Yuki Inoue, Masaaki Hirayama, Naoki Matsui, Masaaki Hirayama, Masaaki Hirayama

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  4. Cubic Rocksalt Li2SnS3 and a Solid Solution with Li3NbS4 Prepared by Mechanochemical Synthesis

    Electrochemistry · 2017-01-01

    Atsushi Sakuda, Kentaro Kuratani, Tomonari Takeuchi, Hisao Kiuchi, Tomoya Kawaguchi, Masahiro Shikano, Hikarí Sakaebe, H. Kobayashi

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  5. Room‐Temperature Synthesis of Three Compounds Featuring the [Ge4S10]4– Anion from a Water‐Soluble Thiogermanate Precursor

    European Journal of Inorganic Chemistry · 2017-08-31

    Felix Danker, Christian Näther, Florian Pielnhofer, Wolfgang Bensch

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  6. Cathode materials and sulfide solid electrolytes for lithium battery

    Unknown journal · 2017-11-20

    Yanghai Xu

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  7. Appearance of Lithium-Ion Conduction in a La–Li–Co–O Band Insulator: Possible Route to Oxide Electrolyte

    ACS Applied Energy Materials · 2018-05-25

    Tsuyoshi Takami, Yoshiyuki Morita, Masao Yonemura, Yoshihisa Ishikawa, Shingo Tanaka, Masahiro Mori, Toshiharu Fukunaga, Eiichiro Matsubara

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  8. Mechanochemical Synthesis and Characterization of Metastable Hexagonal Li4SnS4 Solid Electrolyte

    Inorganic Chemistry · 2018-08-09

    Kento Kanazawa, So Yubuchi, Chie Hotehama, Misae Otoyama, Seiya Shimono, Hiroki Ishibashi, Yoshiki Kubota, Atsushi Sakuda, Akitoshi Hayashi, Masahiro Tatsumisago

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  9. Lithium Transport in Li4.4 M 0.4 M ′0.6S4 (M = Al3+, Ga3+, and M ′ = Ge4+, Sn4+): Combined Crystallographic, Conductivity, Solid State NMR, and Computational Studies

    Chemistry of Materials · 2018-09-13

    Bernhard T. Leube, Kenneth K. Inglis, Elliot J. Carrington, Paul M. Sharp, J. Felix Shin, Alex Ryan Neale, Troy D. Manning, Michael J. Pitcher, Laurence J. Hardwick, Matthew Stephen Dyer, Frédéric Blanc, John B. Claridge, Matthew J. Rosseinsky

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  10. Influence of the Lithium Substructure on the Diffusion Pathways and Transport Properties of the Thio-LISICON Li 4 Ge 1– x Sn x S 4

    Chemistry of Materials · 2019-04-25

    Nicolò Minafra, Sean P. Culver, Cheng Li, Anatoliy Senyshyn, Wolfgang G. Zeier

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  11. Li4-Sb Sn1-S4 solid solutions for air-stable solid electrolytes

    Journal of Energy Chemistry · 2019-05-29

    Zhuoran Zhang, Jianxing Zhang, Yulong Sun, Huanhuan Jia, Linfeng Peng, Yunyang Zhang, Jia Le Xie

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  12. Phase Stability and Electronic Structure of Tin Sulfide Compounds for Li-ion Batteries

    The Journal of Physical Chemistry C · 2019-09-17

    Farnaz Kaboudvand, Julija Vinckevičiu̅tė, Sanjeev Krishna Kolli, Maxwell D. Radin, Anton Van der Ven

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  13. Materials design of ionic conductors for solid state batteries

    Progress in Energy · 2020-02-07

    Saneyuki Ohno, Ananya Banik, Georg F. Dewald, Marvin A. Kraft, Thorben Krauskopf, Nicolò Minafra, Paul S. Till, Manuel Weiß, Wolfgang G. Zeier

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  14. All-solid-state lithium batteries enabled by sulfide electrolytes: from fundamental research to practical engineering design

    Energy & Environmental Science · 2021-01-01

    Changhong Wang, Jianwen Liang, Yang Zhao, Matthew Liu Zheng, Xiaona Li, Xueliang Andy Sun

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  15. Impact of hydration on ion transport in Li 2 Sn 2 S 5 · x H 2 O

    Journal of Materials Chemistry A · 2021-01-01

    Markus Joos, Christian Schneider, Andreas Münchinger, Igor L. Moudrakovski, Robert E. Usiskin, Joachim Maier, Bettina Valeska Lotsch

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  16. Ternary alkali ion thiogallates, A 5 GaS 4 (A = Li and Na), with isolated tetrahedral building units and their ionic conductivities

    Dalton Transactions · 2021-01-01

    Srikanth Balijapelly, Prashanth Sandineni, Amit Adhikary, Nikolay Gerasimchuk, Aleksandr Chernatynskiy, Amitava Choudhury

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  17. Two-Dimensional Substitution: Toward a Better Understanding of the Structure–Transport Correlations in the Li-Superionic Thio-LISICONs

    Chemistry of Materials · 2021-01-04

    Nicolò Minafra, Katharina Hogrefe, Federico Barbon, Bianca Helm, Cheng Li, Martin Wilkening, Wolfgang G. Zeier

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  18. Tracking Ions the Direct Way: Long-Range Li+ Dynamics in the Thio-LISICON Family Li4MCh4 (M = Sn, Ge; Ch = S, Se) as Probed by 7Li NMR Relaxometry and 7Li Spin-Alignment Echo NMR

    The Journal of Physical Chemistry C · 2021-01-21

    Katharina Hogrefe, Nicolò Minafra, Wolfgang G. Zeier, Martin Wilkening

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  19. Insights into the Electrochemical Stability and Lithium Conductivity of Li4MS4 (M = Si, Ge, and Sn)

    ACS Applied Materials & Interfaces · 2021-04-21

    Fengjiao Chen, Songqi Cheng, Jianbo Liu, Shunning Li, Wenhong Ouyang, Baixin Liu

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  20. Progress in thermal stability of all‐solid‐state‐Li‐ion‐batteries

    InfoMat · 2021-06-29

    Yujing Wu, Shuo Wang, Hong Li, Liquan Chen, Fan Bean Wu

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  21. Lithium phosphosulfide electrolytes for solid-state batteries: Part I

    Functional Materials Letters · 2022-07-01

    Xin Lu, Chih‐Long Tsai, Shicheng Yu, Hongying He, Osmane Camara, Hermann Tempel, Zigeng Liu, Anna Windmüller, Evgeny V. Alekseev, Shibabrata Basak, Li Lü, Rüdiger‐A. Eichel, Hans Kungl

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  22. Mechanical Properties of Solid State Li-Ion Batteries

    Elsevier eBooks · 2022-08-27

    Oluwaseun K. Oyewole, Adri Huda, Ridwan A. Ahmed, Deborah O. Oyewole, Nnaemeka Ebechidi, Tofunmi Ogunfunmi, Reisya Ichwani, Abdulhakeem Bello, Winston Oluwole Soboyejo

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  23. Thermal Stability between Sulfide Solid Electrolytes and Oxide Cathode

    ACS Nano · 2022-10-11

    Shuo Wang, Yujing Wu, Tenghuan Ma, Liquan Chen, Hong Li, Fan Bean Wu

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  24. Determination of Gibbs Free Energy in the Compound Formation of Li-P and Li-Fe-O by Pymatgen

    Kaunia Integration and Interconnection Islam and Science · 2022-11-22

    Anis Yuniati, Syamsul Andry

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  25. Current Status and Future Directions in Environmental Stability of Sulfide Solid-State Electrolytes for All-Solid-State Batteries

    Energy Material Advances · 2023-01-01

    Jianwen Liang, Xiaona Li, Changhong Wang, Jung Tae Kim, Rong Yang, Jiantao Wang, Xueliang Andy Sun

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  26. Enhanced Li-Ion Conductivity and Air Stability of Sb-Substituted Li4GeS4 toward All-Solid-State Li-Ion Batteries

    ACS Applied Energy Materials · 2023-05-04

    Jihun Roh, Jeyne Lyoo, Seung‐Tae Hong

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  27. EwaldSolidSolution: A High-Throughput Application to Quickly Sample Stable Site Arrangements for Ionic Solid Solutions

    The Journal of Physical Chemistry A · 2023-06-29

    Seong‐Hoon Jang, Randy Jalem, Yoshitaka Tateyama

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  28. Li-Ion Conductivity of Single-Step Synthesized Glassy-Ceramic Li10GeP2S12 and Post-heated Highly Crystalline Li10GeP2S12

    ACS Applied Materials & Interfaces · 2023-07-13

    Xin Lu, Anna Windmüller, Dana Schmidt, Sandro Schöner, Chih‐Long Tsai, Hans Kungl, Xunfan Liao, Yiwang Chen, Shicheng Yu, Hermann Tempel, Rüdiger‐A. Eichel

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  29. Matching strategy between sulfide solid electrolyte and various anodes: electrolyte modification, interface engineering and electrode structure design

    Energy storage materials · 2024-04-20

    Zhipeng Zhang, Lu Gao, Xiaobin Sun, Nanping Deng, Yixia Zhao, Weimin Kang

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  30. An ab initio study on the elasticity and optical features of semiconductor lithium-based germanate chalcogenides (Li8GeS6 and Li8GeSe6)

    Physica B Condensed Matter · 2024-12-17

    Buğra Yıldız, Aytaç Erkişi

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  31. From non-innocent ionic liquids to reactive agents in the synthesis of chalcogenido metalate compounds

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  32. Dimensional Reduction Guides Electronic Structure Evolution in the A n Cu 4– n SnS 4 Semiconductor Series

    Journal of the American Chemical Society · 2025-08-07

    Michael A. Viti, Zhi Li, Chris M. Wolverton, Mercouri G. Kanatzidis

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  33. Structure and Transport Properties in the Pseudobinary Phase System Li4SiS4–Li4SnS4

    Chemistry of Materials · 2025-08-15

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  34. Establishement of generalized empirical force-fields for sulfide glasses and crystals used as superionic electrolytes in all-solid-state batteries

    Journal of Non-Crystalline Solids · 2025-09-08

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  35. Mechanistic Understanding of Thermal Stability and Safety in Lithium Metal Batteries

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  36. Investigation of the Crystal‐Structure‐Dependent Moisture Stability of the Sulfide Solid Electrolyte Li 4 SnS 4

    European Journal of Inorganic Chemistry · 2025-12-25

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  37. Bridging chemistry and composition-space exploration: Particle swarm optimization of multicomponent glassy sulfide electrolytes

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  38. Anion Engineering of Sulfide Solid Electrolytes: From Fundamentals to High‐Performance All‐Solid‐State Batteries

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  39. Lithium Makes the Difference─Evolution of Lithium Vacancy Disorder during Temperature-Induced Phase Transitions of the Li-Ion Conductor Li4SnS4

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