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RESEARCH PAPER · Chemistry of Materials · 2011

Identification and Quantification of Defects in the Cation Ordering in Mg/Al Layered Double Hydroxides

Sylvian Cadars, Géraldine Layrac, Corine Gérardin, Michaël Deschamps, Jonathan R. Yates, Didier Tichit, Dominique Massiot A

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Identification and Quantification of Defects in the Cation Ordering in Mg/Al Layered Double HydroxidesOriginalApplications of high-resolution 1H solid-state NMR328Anion and Cation Order in Iodide-Bearing Mg/Zn–Al Layered Double Hydroxides47Control of Surface Defects and Agglomeration Mechanism of Layered Double Hydroxide Nanoparticles50Identification of Cation Clustering in Mg–Al Layered Double Hydroxides Using Multinuclear Solid State Nuclear Magnetic Resonance Spectroscopy118Structural Cohesion of M II -M III Layered Double Hydroxides Crystals: Electrostatic Forces and Cationic Polarizing Power58Intercalation of cobalt(II)-tetraphenylporphine tetrasulfonate complex in magnetic NiFe-layered double hydroxide36New Insights into the Molecular Structures, Compositions, and Cation Distributions in Synthetic and Natural Montmorillonite Clays97First-Principles Calculation of NMR Parameters Using the Gauge Including Projector Augmented Wave Method: A Chemist’s Point of View562Synthesis of nano-sized spherical Mg3Al–CO3 layered double hydroxide as a high-temperature CO2 adsorbent143Coupling physical chemical techniques with hydrotalcite-like compounds to exploit their structural features and new multifunctional hybrids with luminescent properties24Layered Double Hydroxides (LDH)235Multinuclear solid-state NMR spectroscopy of a paramagnetic layered double hydroxide20Nuclear Magnetic Resonance Spectroscopy11Locale structure around heteroatoms in alumino- and borosilicates for catalysis1Topological, Geometric, and Chemical Order in Materials: Insights from Solid-State NMR78Abnormally Large Thermal Vibration of Chloride Anions Incorporated in Layered Double Hydroxide Consisting of Mg and Al (Mg/Al = 2)9Interplay between Chemical Composition and Cation Ordering in the Magnetism of Ni/Fe Layered Double Hydroxides70Mid- and near-infrared spectroscopic investigation of homogeneous cation distribution in MgxZnyAl(x+y)/2-layered double hydroxide (LDH)28Applications versus properties of Mg–Al layered double hydroxides provided by their syntheses methods: Alkoxide and alkoxide-free sol–gel syntheses and hydrothermal precipitation118Recent NMR developments applied to organic–inorganic materials89Investigating Local Structure in Layered Double Hydroxides with 17O NMR Spectroscopy42Sorption of borate onto layered double hydroxides assembled on filter paper through in situ hydrothermal crystallization6Alkoxide-intercalated CoFe-layered double hydroxides as precursors of colloidal nanosheet suspensions: structural, magnetic and electrochemical properties130Structural characterisation of a layered double hydroxide nanosheet46Ultrafast Magic Angle Spinning Nuclear Magnetic Resonance57Probing Local Structure of Layered Double Hydroxides with 1H Solid-State NMR Spectroscopy on Deuterated Samples21Relative Humidity-Induced Reversible Hydration Of Sulfate-Intercalated Layered Double Hydroxides21Density functional theory in the solid state400Fabrication of NiFe layered double hydroxides using urea hydrolysis—Control of interlayer anion and investigation on their catalytic performance39Catalytic applications of layered double hydroxides: recent advances and perspectives1762Local environment and composition of magnesium gallium layered double hydroxides determined from solid-state 1H and 71Ga NMR spectroscopy16Long- and Short-Range Constraints for the Structure Determination of Layered Silicates with Stacking Disorder27Stimuli-responsive hybrid materials: breathing in magnetic layered double hydroxides induced by a thermoresponsive molecule43Preparation and catalytic applications of nanomaterials: a review320Intercalation of Benzoxaborolate Anions in Layered Double Hydroxides: Toward Hybrid Formulations for Benzoxaborole Drugs43Dehydration and Dehydroxylation of Layered Double Hydroxides: New Insights from Solid-State NMR and FT-IR Studies of Deuterated Samples53NMR and computational molecular modeling studies of mineral surfaces and interlayer galleries: A review4017O solid-state NMR studies of oxygen-containing catalysts27Evaluation of IN SITU synthesis route of layered hydroxides in the presence of amphiphilic polymers in comparison with their corresponding physical mixtures0How the Method of Synthesis Governs the Local and Global Structure of Zinc Aluminum Layered Double Hydroxides104Theoretical studies of structure and racemization mechanism of aspartate-intercalated hydrotalcite1Improved sensitivity via layered-double-hydroxide-uniformity-dependent chemiluminescence9Modern solid state NMR techniques and concepts in structural studies of synthetic polymers14Supercell program: a combinatorial structure-generation approach for the local-level modeling of atomic substitutions and partial occupancies in crystals543Hierarchical layered double hydroxide epitaxially grown on vermiculite for Cr(VI) removal37Jumping Diffusion of Water Intercalated in Layered Double Hydroxides24A solid state NMR study of layered double hydroxides intercalated with para-amino salicylate, a tuberculosis drug24NiFe‐Based (Oxy)hydroxide Catalysts for Oxygen Evolution Reaction in Non‐Acidic Electrolytes1039Enhanced green fluorescence protein/layered double hydroxide composite ultrathin films: bio-hybrid assembly and potential application as a fluorescent biosensor29Intercalation and structural aspects of macroRAFT agents into MgAl layered double hydroxides14Exploiting NMR spectroscopy for the study of disorder in solids95Carbonate–Hydrogenocarbonate Coexistence and Dynamics in Layered Double Hydroxides35Probing the Dynamics of Layered Double Hydroxides by Solid-State 27Al NMR Spectroscopy16Antioxidant intercalated hydrocalumite as multifunction nanofiller for Poly(propylene): Synthesis, thermal stability, light stability, and anti-migration property24Modeling short-range substitution order and disorder in crystals: Application to the Ga/Si distribution in a natrolite zeolite14Influence on the Electrocatalytic Water Oxidation of M2+/M3+ Cation Arrangement in NiFe LDH: Experimental and Theoretical DFT Evidences20Layered Double Hydroxides: Structure–Property Relationships6Structure and Dynamics of Nonionic Surfactant Aggregates in Layered Materials31Filler-matrix interaction in sodium montmorillonite-organosilica nanocomposite coatings for corrosion protection13The Important Role of Layered Double Hydroxides in Soil Chemical Processes and Remediation: What We Have Learned Over the Past 20 Years42DFT calculations for structural prediction and applications of intercalated lamellar compounds19Aqueous immiscible layered double hydroxides – AIM-LDHs7The distribution of reactive Ni 2+ in 2D Mg 2−x Ni x Al-LDH nanohybrid materials determined by solid state 27 Al MAS NMR spectroscopy15New insight into the preferred valency of interlayer anions in hydrotalcite-like compounds: The effect of Mg/Al ratio57Deciphering the Role of Dipolar Interactions in Magnetic Layered Double Hydroxides31Structural Memory Effect of Mg–Al and Zn–Al layered Double Hydroxides in the Presence of Different Natural Humic Acids: Process and Mechanism107Probing local structure of paramagnetic Ni-Al layered double hydroxides with solid-state 2H NMR spectroscopy16Influences of Cation Ratio, Anion Type, and Water Content on Polytypism of Layered Double Hydroxides38Peptide Formation on Layered Mineral Surfaces: The Key Role of Brucite-like Minerals on the Enhanced Formation of Alanine Dipeptides16Synthesis and characterization of AMO LDH-derived mixed oxides with various Mg/Al ratios as acid–basic catalysts for esterification of benzoic acid with 2-ethylhexanol113Defective and ultrathin NiFe LDH nanosheets decorated on V-doped Ni 3 S 2 nanorod arrays: a 3D core–shell electrocatalyst for efficient water oxidation229Investigation of the surface confinement effect of copper nanoclusters: construction of an ultrasensitive fluorescence turn-on bio-enzyme sensing platform33Hydration and Hydroxylation of MgO in Solution: NMR Identification of Proton-Containing Intermediate Phases28Synthesis and Structural Characterization of a Pure ZnAl 4 (OH) 12 (SO 4 )·2.6H 2 O Layered Double Hydroxide19Uptake of heavy metal ions in layered double hydroxides and applications in cementitious materials: Experimental evidence and first-principle study40Layered Double Hydroxides: A Toolbox for Chemistry and Biology156Hidróxidos duplos lamelares: estudos da intercalação e liberação de N-acetil-L-cisteína0Unraveling Gibbsite Transformation Pathways into LiAl-LDH in Concentrated Lithium Hydroxide85Atomic Level Understanding of Orthophosphate Adsorption by Magnesium Aluminum-Layered Double Hydroxides—A Multitechnique Study45Favorable Intercalation of Nitrate Ions with Fluorine-Substituted Layered Double Hydroxides21Effects of Cu 2+ incorporation on ZnAl-layered double hydroxide37Imparting CO 2 reduction selectivity to ZnGa 2 O 4 photocatalysts by crystallization from hetero nano assembly of amorphous-like metal hydroxides24t 1 -Noise eliminated dipolar heteronuclear multiple-quantum coherence solid-state NMR spectroscopy51Intercalation of (η5‐Pentamethylcyclopentadienyl)trioxomolybdenum(VI) in a Layered Double Hydroxide3Periodic DFT Calculations—Review of Applications in the Pharmaceutical Sciences99Integrated glycerol- and ethanol-based chemical synthesis routes using Cu–Mg–Al LDH-derived catalysts without external hydrogen: Intervention of bio-ethanol co-fed with glycerol26Synthesis and Properties of New Multilayer Chitosan@layered Double Hydroxide/Drug Loaded Phospholipid Bilayer Nanocomposite Bio-Hybrids16Thermal Evolution of Natural Layered Double Hydroxides: Insight from Quintinite, Hydrotalcite, Stichtite, and Iowaite as Reference Samples for CO3- and Cl-Members of the Hydrotalcite Supergroup2489 Y chemical shift anisotropy: a sensitive structural probe of layered yttrium hydroxides revealed by solid-state NMR spectroscopy and DFT calculations9Solid state NMR studies of layered double hydroxides16Review for "35 Cl ‐ 1 H Heteronuclear Correlation MAS NMR Experiments for Probing Pharmaceutical Salts"0“X Factor” in the Structure and Anion Exchange of Layered Yttrium Hydroxides15Pt atomic clusters catalysts with local charge transfer towards selective oxidation of furfural108Perspectives on Multifunctional Catalysts Derived from Layered Double Hydroxides toward Upgrading Reactions of Biomass Resources86Review for "35 Cl ‐ 1 H Heteronuclear Correlation MAS NMR Experiments for Probing Pharmaceutical Salts"0Decision letter for "35 Cl ‐ 1 H Heteronuclear Correlation MAS NMR Experiments for Probing Pharmaceutical Salts"0NMR Crystallography Reveals Carbonate Induced Al‐Ordering in ZnAl Layered Double Hydroxide17Enhanced Fluoride Uptake by Layered Double Hydroxides under Alkaline Conditions: Solid-State NMR Evidence of the Role of Surface >MgOH Sites55Efficient, scalable, closed-loop synthesis of highly crystalline pure phase MgAl-layered double hydroxides intercalated with hydroxyl anions11Towards understanding photon absorption and emission in MgAl layered double hydroxide22Long-Range and Short-Range Structures of Multimetallic Layered Double Hydroxides28Characterization of Monochromate and Hemichromate AFm Phases and Chromate-Containing Ettringite by 1H, 27Al, and 53Cr MAS NMR Spectroscopy5Effects of the cation ordering in Mg:Al and Zn:Al layered double hydroxides on crystallographic and spectroscopical properties by means of first principles calculations13Impact of Synthesis Method and Metal Salt Precursors on the CO2 Adsorption Performance of Layered Double Hydroxides Derived Mixed Metal Oxides13A green route for the preparation of layered double hydroxides from basic magnesium carbonate8Efficient removal of glyphosate from aqueous solutions by adsorption on Mg–Al-layered double oxides: thermodynamic, kinetic, and mechanistic investigation22Engineering Heterostructures of Layered Double Hydroxides and Metal Nanoparticles for Plasmon-Enhanced Catalysis11Insights into memory effect mechanisms of layered double hydroxides with solid-state NMR spectroscopy125Advances in the characterization of inorganic solids using NMR correlation experiments6Expanding the gallery of solvent-free nanofluids: Using layered double hydroxides as core nanostructures21Semi-quantitative determination of active sites in heterogeneous catalysts for photo/electrocatalysis26Two‐dimensional Pure Isotropic Proton Solid State NMR17Two‐dimensional Pure Isotropic Proton Solid State NMR0Active-learning search for unitcell structures: A case study on Mg3Bi2-xSbx13Enhanced adsorption effect of defect ordering Mg/Al on layered double hydroxides nanosheets with highly efficient removal of Congo red17A solid-state NMR method for characterization of pharmaceutical eutectics7Insights into the Structure of Sucralfate by Advanced Solid- and Liquid-State NMR2Interplay between Defects and Short-Range Disorder Manipulating the Oxygen Evolution Reaction on a Layered Double Hydroxide Electrocatalyst17Recent advances of metal vacancies in energy and environmental catalysis: Synthesis, characterization, and roles44Full valorisation of waste PET into dimethyl terephthalate and cyclic arylboronic esters61Influence of the Alumina Interface layer in Silica@Layered Double Hydroxide Core–Shell Particles8Influence of phosphates on phase formation in alkali‐activated MgO‐Al2O3‐SiO2‐P2O5 cements4Influence of Al-clustering in the catalytic activity of layered double hydroxides for the Baeyer-Villiger oxidation4Pyroaurite-like phases (Mg-Fe3+ LDH) synthesis and solubility19Disorder in Inorganic Materials1Characterization of aqueous carbonated cement-based materials by multinuclear solid-state NMR spectroscopy6Atomic‐Scale Regulation of Covalent Bonding for Blue Phosphorescence4Magnesium-based nanomaterials for cancer therapy: Unraveling mechanisms and current developments4Eco-friendly synthesis of ultrathin Mg/Al layered double hydroxides with high specific surface area with minimal water content2Regenerable Water Remediation Platform for Ultrafast Capture and Mineralization of Per‐ and Polyfluoroalkyl Substances3129Xe NMR spectroscopy of paramagnetic Mg2-Ni Al layered double hydroxides1Interplay between defects, disorder and flexibility in layered double hydroxides0Interplay between defects, disorder and flexibility in layered double hydroxides2The hydrogen network in kaolinite and tetracalcium monocarboaluminate hydrate from 1H MAS NMR at very high magnetic field and spinning frequencies0

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  47. A solid state NMR study of layered double hydroxides intercalated with para-amino salicylate, a tuberculosis drug

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  48. NiFe‐Based (Oxy)hydroxide Catalysts for Oxygen Evolution Reaction in Non‐Acidic Electrolytes

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  49. Enhanced green fluorescence protein/layered double hydroxide composite ultrathin films: bio-hybrid assembly and potential application as a fluorescent biosensor

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  50. Intercalation and structural aspects of macroRAFT agents into MgAl layered double hydroxides

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