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RESEARCH PAPER · Dalton Transactions · 2004

Oxygen and nitrogen Lewis base adducts of [UO2(OTf)2]. Crystal structures of polypyridine complexes with out-of-plane uranyl equatorial coordination

J.‐C. Berthet, M. Nierlich, M. Ephritikhine

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Oxygen and nitrogen Lewis base adducts of [UO2(OTf)2]. Crystal structures of polypyridine complexes with out-of-plane uranyl equatorial coordinationOriginal16 Scandium, yttrium, the lanthanides and the actinides5Unprecedented reduction of the uranyl ion [UO2]2+ into a polyoxo uranium(iv) cluster: Synthesis and crystal structure of the first f-element oxide with a M6(µ3-O)8 core73Versatile new uranyl(vi) dihalide complexes supported by tunable organic amide ligands19Lanthanide( III )/Actinide( III ) Differentiation in the Cerium and Uranium Complexes [M(C5Me5)2(L)]0,+ (L=2,2′‐Bipyridine, 2,2′:6′,2′′‐Terpyridine): Structural, Magnetic, and Reactivity Studies108Syntheses and photoluminescent properties of two uranyl-containing compounds with extended structures98Easy access to stable pentavalent uranyl complexes98The vitality of uranium molecular chemistry at the dawn of the XXIst century314Uranyl pyridine-dicarboxylate compounds with clustered water molecules67Fluoride Abstraction and Reversible Photochemical Reduction of Cationic Uranyl(VI) Phosphine Oxide Complexes44Stable analogs of the uranyl ion containing 1,1,3,3-tetramethylguanidine8Synthesis, crystal structure and optical properties of [Ag(UO2)3(OAc)9][Zn(H2O)4(CH3CH2OH)2]: A novel compound containing closed-shell 3d10, 4d10 and 5d10 metal ions31The first cyclopentadienyl complex of uranyl61Coordination and extraction studies of an unexplored bi-functional ligand, carbamoyl methyl pyrazole (CMPz) with uranium(VI), lanthanum(III) and cerium(III) nitrates19Synthesis and crystal structure of [UO2(BH4)2(hmpa)2], a novel uranyl complex and the first metal oxoborohydride15Highlights in Uranium Coordination Chemistry59Imidazo[4,5-f]-1,10-phenanthrolines: Versatile Ligands for the Design of Metallomesogens97Sterically Congested Uranyl Complexes with Seven-Coordination of the UO2 Unit: the Peculiar Ligation Mode of Nitrate in [UO2(NO3)2(Rbtp)] Complexes65Mixed-Ligand Uranyl(V) β-Diketiminate/β-Diketonate Complexes: Synthesis and Characterization64Coordination of bistriflimide and triflate to the uranyl bis(diphenylphosphino)methane dication, {UO2(DPPMO2)2}2+17Uranyl ion complexes of cucurbit[7]uril with zero-, one- and two-dimensionality62Exploring the Effects of Reduction or Lewis Acid Coordination on the U═O Bond of the Uranyl Moiety84Oxo ligand functionalization in the uranyl ion (UO22+)335Coordination of N-Donor Ligands to a Uranyl(V) β-Diketiminate Complex45Comparative investigation of the solution species [U(CO3)5]6− and the crystal structure of Na6[U(CO3)5]·12H2O53Investigating the electronic structure and bonding in uranyl compounds by combining NEXAFS spectroscopy and quantum chemistry42Linear uranium metallocenes with polydentate aromatic nitrogen ligands18Density Functional Analysis of the Trigonal Uranyl Equatorial Coordination in Hexahomotrioxacalix[3]arene-based Macrocyclic Complexes18Binuclear Uranium(VI) Complexes with a “Pacman” Expanded Porphyrin: Computational Evidence for Highly Unusual Bis‐Actinyl Structures45Di-2-pyridyl ketone in actinide chemistry: Dinuclear uranyl complexes16A new clover-shaped trinuclear uranium(VI) complex: Synthesis, structure and photoluminescence property26Binuclear Hexa- and Pentavalent Uranium Complexes with a Polypyrrolic Ligand: A Density Functional Study of Water- and Hydronium-Induced Reactions44Competitive Complexation of Nitrates and Chlorides to Uranyl in a Room Temperature Ionic Liquid40Uranyl(VI)–Acetylacetonate Coordination Compounds with Various N-Heterocyclic Ligands16Tetrameric entity resulting from two distinct dinuclear uranyl-centered motifs bridged through μ2-OH and pyridazine-3,6-dicarboxylate26Probing the local coordination environment and nuclearity of uranyl(vi) complexes in non-aqueous media by emission spectroscopy109Coordination chemistry of pyrazolone based Schiff bases relevant to uranyl sequestering agents: Synthesis, characterization and 3D molecular modeling of some octa-coordinate mono- and binuclear-dioxouranium(VI) complexes12Exploring the Uranyl Organometallic Chemistry: From Single to Double Uranium−Carbon Bonds135Facile Reduction of a Uranyl(VI) β-Ketoiminate Complex to U(IV) Upon Oxo Silylation623D-supermolecular structure and electronic absorption of uranyl β-diketone [UO2(tfa)2(L)] (L=H2O, OHCH2CH3) complex10Bis(methanol-κO)dioxido[3,3′-(1H-1,2,4-triazole-3,5-diyl)diphenolato-κ3O,N4,O′]uranium(VI) methanol monosolvate4Steric Effects on Uranyl Complexation: Synthetic, Structural, and Theoretical Studies of Carbamoyl Pyrazole Compounds of the Uranyl(VI) Ion25Nitrogen-rich Compounds of the Actinoids: Dioxouranium(VI) 5,5′-Azobis[tetrazolide] Pentahydrate and Its Unusually Small Uranyl Angle13Structural Versatility of Uranyl(VI) Nitrate Complexes That Involve the Diamide Ligand Et2N(C=O)(CH2)n(C=O)NEt2 (0 ≤ n ≤ 6)29Coordination of 1,10-phenanthroline, 3,4,7,8-tetramethyl-1,10-phenanthroline and 2,4,6-tris(2-pyridyl)-1,3,5-triazine to MX3 (M=Ce, U; X=I, OSO2CF3) in pyridine and acetonitrile9Bisactinyl halogenated complexes: relativistic density functional theory calculation and experimental synthesis9New Reactivity of the Uranyl(VI) Ion116Crystal structures of 2,2′:6′,2″-terpyridine uranyl chlorides molecular assemblies and their luminescence signatures24Synthesis, Structures, and Luminescent Properties of Uranyl Terpyridine Aromatic Carboxylate Coordination Polymers85Actinide oxalates, solid state structures and applications160Thorocene adducts of the neutral 2,2′-bipyridine and its radical anion. Synthesis and crystal structures of [Th(η8-C8H8)2(κ2-bipy)] and [Th(μ-η8:η5-C8H8)2(κ2-bipy)K(py)2]∞25Toward Equatorial Planarity about Uranyl: Synthesis and Structure of Tridentate Nitrogen-Donor {UO2}2+ Complexes17Synthetic, structural, extraction and theoretical studies of uranyl nitrate dithio-diglycolamide compounds11Structural/electronic properties and reaction energies of a series of mono- and bis-uranyl dihalides equatorially coordinated by N/O ligands1Novel uranyl( vi ) complexes incorporating propylene-bridged salen-type N 2 O 2 -ligands: a structural and computational approach50Reductive Silylation of the Uranyl Ion with Ph3SiOTf23Combining coordination and supramolecular chemistry to explore uranyl assembly in the solid state51Synthesis, Characterization, and Crystal Structure of New Complex, Based on Proton Transfer to Uranium(VI) Complex3Steric effects in complexes of diphenyl(2-pyridyl)phosphine oxide with the uranyl ion. Synthetic, structural and theoretical studies10Crystal structure of μ-peroxido-κ4O1,O2:O1′,O2′-bis[(nitrato-κO)(2,2′:6′,2′′-terpyridine-κ3N,N′,N′′)dioxidouranium(VI)]3Role of N-Donor Sterics on the Coordination Environment and Dimensionality of Uranyl Thiophenedicarboxylate Coordination Polymers53Probing the Influence of N‐Donor Capping Ligands on Supramolecular Assembly in Molecular Uranyl Materials45Anchoring flexible uranyl dicarboxylate chains through stacking interactions of ancillary ligands on chiral U( vi ) centres37Relativistic DFT and experimental studies of mono- and bis-actinyl complexes of an expanded Schiff-base polypyrrole macrocycle19Perturbation of the O–U–O Angle in Uranyl by Coordination to a 12-Membered Macrocycle32Pseudo-halide uranyl salicylaldiminate complexes including the isolation of a rare uranyl azide3Novel Uranyl Coordination Polymers Based on Quinoline-Containing Dicarboxylate by Altering Auxiliary Ligands: From 1D Chain to 3D Framework31A computational investigation of polypyrrolic macrocyclic actinyl complexes: effects of explicit solvent coordination on structure, vibrational spectra and redox property9Harnessing uranyl oxo atoms via halogen bonding interactions in molecular uranyl materials featuring 2,5-diiodobenzoic acid and N-donor capping ligands39Complexation of actinides Am(III), Th(IV), Pu(IV) and U(VI) with poly-N-dentate ligands SO3-Ph-BTP and SO3-Ph-BTBP0F-element metalated dipyrrins: synthesis and characterization of a family of uranyl bis(dipyrrinate) complexes12Coordination Characteristics of Uranyl BBP Complexes: Insights from an Electronic Structure Analysis6Uranyl-tri-bis(silyl)amide Alkali Metal Contact and Separated Ion Pair Complexes17Bis(hydroxylamino)triazines: High Selectivity and Hydrolytic Stability of Hydroxylamine-Based Ligands for Uranyl Compared to Vanadium(V) and Iron(III)15Applications of boroxide ligands in supporting small molecule activation by U( iii ) and U( iv ) complexes13Catalyseurs d’hydrosilylation pour la réduction de liaisons C-O dans les polymères oxygénés0A combined experimental and quantum chemical studies on the structure and binding preferences of picolinamide based ligands with uranyl nitrate4Breaking C–O Bonds with Uranium: Uranyl Complexes as Selective Catalysts in the Hydrosilylation of Aldehydes40Synthesis, Spectral and Thermal Properties of Hydrazinium, Aminoguanidinium and Pyridinium Uranyl Pyridine-2,6-Dicarboxylates0Ultrasonication-driven downscaling and formation of Lewis acid–base sites in hydrogen-bonded Co metal–organic frameworks trigger exceptional catalytic performance for the Knoevenagel condensation reaction7Neptunium(V) N,N′-dicyanoguanidinate complexes with electroneutral N-donor ligands2Reactions of U(DMSO) 8 (ClO 4 ) 4 with Terpyridine Yield Dimeric Hydrolysis Products and Induce C–C Coupling0

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  1. 16 Scandium, yttrium, the lanthanides and the actinides

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  2. Unprecedented reduction of the uranyl ion [UO2]2+ into a polyoxo uranium(iv) cluster: Synthesis and crystal structure of the first f-element oxide with a M6(µ3-O)8 core

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  3. Versatile new uranyl(vi) dihalide complexes supported by tunable organic amide ligands

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  4. Lanthanide( III )/Actinide( III ) Differentiation in the Cerium and Uranium Complexes [M(C5Me5)2(L)]0,+ (L=2,2′‐Bipyridine, 2,2′:6′,2′′‐Terpyridine): Structural, Magnetic, and Reactivity Studies

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  5. Syntheses and photoluminescent properties of two uranyl-containing compounds with extended structures

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  6. Easy access to stable pentavalent uranyl complexes

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  7. The vitality of uranium molecular chemistry at the dawn of the XXIst century

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  8. Uranyl pyridine-dicarboxylate compounds with clustered water molecules

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  9. Fluoride Abstraction and Reversible Photochemical Reduction of Cationic Uranyl(VI) Phosphine Oxide Complexes

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  10. Stable analogs of the uranyl ion containing 1,1,3,3-tetramethylguanidine

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  11. Synthesis, crystal structure and optical properties of [Ag(UO2)3(OAc)9][Zn(H2O)4(CH3CH2OH)2]: A novel compound containing closed-shell 3d10, 4d10 and 5d10 metal ions

    Dalton Transactions · 2007-01-01

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  12. The first cyclopentadienyl complex of uranyl

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  13. Coordination and extraction studies of an unexplored bi-functional ligand, carbamoyl methyl pyrazole (CMPz) with uranium(VI), lanthanum(III) and cerium(III) nitrates

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    S. Kannan, J.S. Gamare, K. Venugopal Chetty, Michael G. B. Drew

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  14. Synthesis and crystal structure of [UO2(BH4)2(hmpa)2], a novel uranyl complex and the first metal oxoborohydride

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  15. Highlights in Uranium Coordination Chemistry

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  16. Imidazo[4,5-f]-1,10-phenanthrolines: Versatile Ligands for the Design of Metallomesogens

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    Thomas Cardinaels, Jan Ramaekers, Peter Nockemann, Kris Driesen, Kristof Van Hecke, Luc Van Meervelt, Shengbin Lei, Steven De Feyter, Daniel Guillon, Bertrand Donnio, Koen Binnemans

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  17. Sterically Congested Uranyl Complexes with Seven-Coordination of the UO2 Unit: the Peculiar Ligation Mode of Nitrate in [UO2(NO3)2(Rbtp)] Complexes

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  18. Mixed-Ligand Uranyl(V) β-Diketiminate/β-Diketonate Complexes: Synthesis and Characterization

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  19. Coordination of bistriflimide and triflate to the uranyl bis(diphenylphosphino)methane dication, {UO2(DPPMO2)2}2+

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  20. Uranyl ion complexes of cucurbit[7]uril with zero-, one- and two-dimensionality

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  21. Exploring the Effects of Reduction or Lewis Acid Coordination on the U═O Bond of the Uranyl Moiety

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  22. Oxo ligand functionalization in the uranyl ion (UO22+)

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  23. Coordination of N-Donor Ligands to a Uranyl(V) β-Diketiminate Complex

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  24. Comparative investigation of the solution species [U(CO3)5]6− and the crystal structure of Na6[U(CO3)5]·12H2O

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  25. Investigating the electronic structure and bonding in uranyl compounds by combining NEXAFS spectroscopy and quantum chemistry

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  26. Linear uranium metallocenes with polydentate aromatic nitrogen ligands

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  27. Density Functional Analysis of the Trigonal Uranyl Equatorial Coordination in Hexahomotrioxacalix[3]arene-based Macrocyclic Complexes

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  28. Binuclear Uranium(VI) Complexes with a “Pacman” Expanded Porphyrin: Computational Evidence for Highly Unusual Bis‐Actinyl Structures

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  29. Di-2-pyridyl ketone in actinide chemistry: Dinuclear uranyl complexes

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  30. A new clover-shaped trinuclear uranium(VI) complex: Synthesis, structure and photoluminescence property

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  31. Binuclear Hexa- and Pentavalent Uranium Complexes with a Polypyrrolic Ligand: A Density Functional Study of Water- and Hydronium-Induced Reactions

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  32. Competitive Complexation of Nitrates and Chlorides to Uranyl in a Room Temperature Ionic Liquid

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  33. Uranyl(VI)–Acetylacetonate Coordination Compounds with Various N-Heterocyclic Ligands

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  34. Tetrameric entity resulting from two distinct dinuclear uranyl-centered motifs bridged through μ2-OH and pyridazine-3,6-dicarboxylate

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  35. Probing the local coordination environment and nuclearity of uranyl(vi) complexes in non-aqueous media by emission spectroscopy

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  36. Coordination chemistry of pyrazolone based Schiff bases relevant to uranyl sequestering agents: Synthesis, characterization and 3D molecular modeling of some octa-coordinate mono- and binuclear-dioxouranium(VI) complexes

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  37. Exploring the Uranyl Organometallic Chemistry: From Single to Double Uranium−Carbon Bonds

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  38. Facile Reduction of a Uranyl(VI) β-Ketoiminate Complex to U(IV) Upon Oxo Silylation

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  39. 3D-supermolecular structure and electronic absorption of uranyl β-diketone [UO2(tfa)2(L)] (L=H2O, OHCH2CH3) complex

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  40. Bis(methanol-κO)dioxido[3,3′-(1H-1,2,4-triazole-3,5-diyl)diphenolato-κ3O,N4,O′]uranium(VI) methanol monosolvate

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  41. Steric Effects on Uranyl Complexation: Synthetic, Structural, and Theoretical Studies of Carbamoyl Pyrazole Compounds of the Uranyl(VI) Ion

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  42. Nitrogen-rich Compounds of the Actinoids: Dioxouranium(VI) 5,5′-Azobis[tetrazolide] Pentahydrate and Its Unusually Small Uranyl Angle

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  43. Structural Versatility of Uranyl(VI) Nitrate Complexes That Involve the Diamide Ligand Et2N(C=O)(CH2)n(C=O)NEt2 (0 ≤ n ≤ 6)

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  44. Coordination of 1,10-phenanthroline, 3,4,7,8-tetramethyl-1,10-phenanthroline and 2,4,6-tris(2-pyridyl)-1,3,5-triazine to MX3 (M=Ce, U; X=I, OSO2CF3) in pyridine and acetonitrile

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  45. Bisactinyl halogenated complexes: relativistic density functional theory calculation and experimental synthesis

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  46. New Reactivity of the Uranyl(VI) Ion

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  47. Crystal structures of 2,2′:6′,2″-terpyridine uranyl chlorides molecular assemblies and their luminescence signatures

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  48. Synthesis, Structures, and Luminescent Properties of Uranyl Terpyridine Aromatic Carboxylate Coordination Polymers

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  49. Actinide oxalates, solid state structures and applications

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  50. Thorocene adducts of the neutral 2,2′-bipyridine and its radical anion. Synthesis and crystal structures of [Th(η8-C8H8)2(κ2-bipy)] and [Th(μ-η8:η5-C8H8)2(κ2-bipy)K(py)2]∞

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