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RESEARCH PAPER · The Journal of Physical Chemistry B · 2001

Piezo X-ray Absorption Spectroscopy for the Investigation of Solid-State Transformations in the Millisecond Range

Jan‐Dierk Grunwaldt, Dirk Lützenkirchen−Hecht, Matthias Richwin, Sven Grundmann, Bjerne S. Clausen, R. Frahm

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Piezo X-ray Absorption Spectroscopy for the Investigation of Solid-State Transformations in the Millisecond RangeOriginalBringing time resolution to EXAFS: recent developments and application to chemical systems112Particle development and characterisation in Pt(acac)2 and Pt(acac)2/GeBu4 derived catalysts supported upon porous and mesoporous SiO2: effect of reductive environment, and support structure20A novel crystal bender for x-ray synchrotron radiation monochromators6Piezo-XAFS–time-resolved x-ray absorption spectroscopy31Time-resolved studies of diffusion via energy dispersive X-ray absorption spectroscopy10Mapping the chemical states of an element inside a sample using tomographic x-ray absorption spectroscopy87Application of time-resolved in-situ X-ray absorption spectroscopy in solid-state chemistry16Recent Developments in the In Situ XAFS and Related Work for the Characterization of Catalysts in Japan11In situ EXAFS study on the oxidation state of Pd/Al2O3 and Bi–Pd/Al2O3 during the liquid-phase oxidation of 1-phenylethanol84X-ray absorption spectroscopy under reaction conditions: suitability of different reaction cells for combined catalyst characterization and time-resolved studies248Time-Scale and Sequence of Dynamic Structural Changes in a MgO-Attached Ruthenium Cluster Catalyst Observed by in Situ Time-Resolved DXAFS32Xray Absorption Spectroscopy on Heterogeneous Catalysts at the new XAS Beamline at ANKA21Applications of X-Ray Absorption Spectroscopy in Materials Science32D-Mapping of the Catalyst Structure Inside a Catalytic Microreactor at Work: Partial Oxidation of Methane over Rh/Al 2 O 3158Combining diffuse reflectance infrared spectroscopy (DRIFTS), dispersive EXAFS, and mass spectrometry with high time resolution: Potential, limitations, and application to the study of NO interaction with supported Rh catalysts77Dynamic adsorbate/reaction induced structural change of supported metal nanoparticles: heterogeneous catalysis and beyond201SCANNING TOMOGRAPHY0A high-temperature furnace forin situsynchrotron X-ray spectroscopy under controlled atmospheric conditions8Catalysts at work: From integral to spatially resolved X-ray absorption spectroscopy100Chapter 6 Characterization of Catalysts in Reactive Atmospheres by X‐ray Absorption Spectroscopy98Structural changes of noble metal catalysts during ignition and extinction of the partial oxidation of methane studied by advanced QEXAFS techniques52Advancing Time-resolved Methods in Monitoring and Characterization of Catalysts13Applying Dynamic and Synchronous DRIFTS/EXAFS to the Structural Reactive Behaviour of Dilute (≤1 wt%) Supported Rh/Al2O3 Catalysts using Quick and Energy Dispersive EXAFS65Reduction and re-oxidation of Cu/Al2O3catalysts investigated with quick-scanning XANES and EXAFS10Shining X-rays on catalysts at work16Hard and soft X-ray microscopy and tomography in catalysis: bridging the different time and length scales181Hydrothermal Synthesis of Bi6S2O15 Nanowires: Structural, in situ EXAFS, and Humidity‐Sensing Studies37Quick-EXAFS implementation on the general purpose EXAFS beamline at ESRF36Nucleation and Aggregative Growth Process of Platinum Nanoparticles Studied by in Situ Quick XAFS Spectroscopy98The chemical sensitivity of X-ray spectroscopy: high energy resolution XANES versus X-ray emission spectroscopy of substituted ferrocenes58QEXAFS in Catalysis Research: Principles, Data Analysis, and Applications8François Garin: Pioneer work in catalysis through synchrotron radiation9X-Ray Absorption and Scattering Methods0Cell Designs for In Situ and Operando Studies22Tracking dynamic structural changes in catalysis by rapid 2D-XANES microscopy14Past, present and future—sample environments for materials research studies in scattering and spectroscopy; a UK perspective3X-Ray Microscopy and Tomography2Operando X-ray absorption fine structure spectroscopy and its applications to catalysts1

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  1. Bringing time resolution to EXAFS: recent developments and application to chemical systems

    Chemical Society Reviews · 2002-01-29

    Mark A. Newton, Andrew J. Dent, John Evans

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  2. Particle development and characterisation in Pt(acac)2 and Pt(acac)2/GeBu4 derived catalysts supported upon porous and mesoporous SiO2: effect of reductive environment, and support structure

    Physical Chemistry Chemical Physics · 2002-01-31

    Steven G. Fiddy, Mark A. Newton, Tom Campbell, Andrew J. Dent, Ian Harvey, Guiseppe Salvini, Sandra Turin, John Evans

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  3. A novel crystal bender for x-ray synchrotron radiation monochromators

    Review of Scientific Instruments · 2002-03-01

    Ralf Zaeper, Matthias Richwin, Dirk Lützenkirchen−Hecht, R. Frahm

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  4. Piezo-XAFS–time-resolved x-ray absorption spectroscopy

    Review of Scientific Instruments · 2002-03-01

    Matthias Richwin, Ralf Zaeper, Dirk Lützenkirchen−Hecht, R. Frahm

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  5. Time-resolved studies of diffusion via energy dispersive X-ray absorption spectroscopy

    Electrochemistry Communications · 2002-12-28

    Rachel L. O’Malley, Antje Vollmer, Jonathan R. I. Lee, Ian Harvey, Jon Headspith, Sofía Díaz‐Moreno, Trevor Rayment

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  6. Mapping the chemical states of an element inside a sample using tomographic x-ray absorption spectroscopy

    Applied Physics Letters · 2003-05-08

    Christian G. Schroer, M. Kuhlmann, Til Florian Günzler, B. Lengeler, Matthias Richwin, B. Griesebock, Dirk Lützenkirchen−Hecht, R. Frahm, Eric Ziegler, Ali Mashayekhi, Dean R. Haeffner, Jan‐Dierk Grunwaldt, Alfons Baiker

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  7. Application of time-resolved in-situ X-ray absorption spectroscopy in solid-state chemistry

    Analytical and Bioanalytical Chemistry · 2003-07-01

    Thorsten Ressler

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  8. Recent Developments in the In Situ XAFS and Related Work for the Characterization of Catalysts in Japan

    Catalysis Surveys from Asia · 2003-09-01

    Kiyotaka Asakura

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  9. In situ EXAFS study on the oxidation state of Pd/Al2O3 and Bi–Pd/Al2O3 during the liquid-phase oxidation of 1-phenylethanol

    Journal of Catalysis · 2003-12-04

    Csilla Keresszegi, Jan‐Dierk Grunwaldt, Tamás Mallát, Alfons Baiker

    Read original paper ↗ ·

  10. X-ray absorption spectroscopy under reaction conditions: suitability of different reaction cells for combined catalyst characterization and time-resolved studies

    Physical Chemistry Chemical Physics · 2004-01-01

    Jan‐Dierk Grunwaldt, Matteo Caravati, Stefan Hannemann, Alfons Baiker

    Read original paper ↗ ·

  11. Time-Scale and Sequence of Dynamic Structural Changes in a MgO-Attached Ruthenium Cluster Catalyst Observed by in Situ Time-Resolved DXAFS

    The Journal of Physical Chemistry B · 2004-04-13

    Akane Suzuki, Aritomo Yamaguchi, Teiji Chihara, Yasuhiro Inada, Makoto Yuasa, Masahiko Abe, Masaharu Nomura, Yasuhiro Iwasawa

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  12. Xray Absorption Spectroscopy on Heterogeneous Catalysts at the new XAS Beamline at ANKA

    Physica Scripta · 2005-01-01

    Jan‐Dierk Grunwaldt, Stefan Hannemann, J. Gttlicher, S. Mangold, Melissa A. Denecke, Alfons Baiker

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  13. Applications of X-Ray Absorption Spectroscopy in Materials Science

    Kluwer Academic Publishers eBooks · 2006-01-12

    Valérie Briois, Christine Giorgetti, F. Baudelet, A.-M. Flank, Miriam Sanae Tokumoto, Sandra H. Pulcinelli, Celso Valentim Santilli

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  14. 2D-Mapping of the Catalyst Structure Inside a Catalytic Microreactor at Work: Partial Oxidation of Methane over Rh/Al 2 O 3

    The Journal of Physical Chemistry B · 2006-04-07

    Jan‐Dierk Grunwaldt, Stefan Hannemann, Christian G. Schroer, Alfons Baiker

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  15. Combining diffuse reflectance infrared spectroscopy (DRIFTS), dispersive EXAFS, and mass spectrometry with high time resolution: Potential, limitations, and application to the study of NO interaction with supported Rh catalysts

    Catalysis Today · 2006-11-21

    Mark A. Newton, Andrew J. Dent, Steven G. Fiddy, Bhrat Jyoti, John Evans

    Read original paper ↗ ·

  16. Dynamic adsorbate/reaction induced structural change of supported metal nanoparticles: heterogeneous catalysis and beyond

    Chemical Society Reviews · 2008-01-01

    Mark A. Newton

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  17. SCANNING TOMOGRAPHY

    Unknown journal · 2008-03-20

    A. Simionovici, P. Bleuet, Bruno Golosio, Christian G. Schroer

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  18. A high-temperature furnace forin situsynchrotron X-ray spectroscopy under controlled atmospheric conditions

    Journal of Synchrotron Radiation · 2008-07-21

    S. G. Eeckhout, B. Gorges, Laurent Barthe, Orietta Pelosi, Оlga V. Safonova, Gabriele Giuli

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  19. Catalysts at work: From integral to spatially resolved X-ray absorption spectroscopy

    Catalysis Today · 2008-12-20

    Jan‐Dierk Grunwaldt, Bertram Kimmerle, Alfons Baiker, Pit Boye, Christian G. Schroer, Pieter Glatzel, Camelia Nicoleta Borca, Felix Beckmann

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  20. Chapter 6 Characterization of Catalysts in Reactive Atmospheres by X‐ray Absorption Spectroscopy

    Advances in catalysis · 2009-01-01

    Simon R. Bare, Thorsten Ressler

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  21. Structural changes of noble metal catalysts during ignition and extinction of the partial oxidation of methane studied by advanced QEXAFS techniques

    Physical Chemistry Chemical Physics · 2009-01-01

    Jan‐Dierk Grunwaldt, Matthias Josef Beier, Bertram Kimmerle, Alfons Baiker, Maarten Nachtegaal, B. Griesebock, Dirk Lützenkirchen−Hecht, Jan Stötzel, R. Frahm

    Read original paper ↗ ·

  22. Advancing Time-resolved Methods in Monitoring and Characterization of Catalysts

    Synchrotron Radiation News · 2009-03-26

    R. Frahm, Jan Stötzel, Dirk Lützenkirchen−Hecht

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  23. Applying Dynamic and Synchronous DRIFTS/EXAFS to the Structural Reactive Behaviour of Dilute (≤1 wt%) Supported Rh/Al2O3 Catalysts using Quick and Energy Dispersive EXAFS

    Topics in Catalysis · 2009-06-23

    Mark A. Newton

    Read original paper ↗ ·

  24. Reduction and re-oxidation of Cu/Al2O3catalysts investigated with quick-scanning XANES and EXAFS

    Journal of Physics Conference Series · 2009-11-01

    Jan Stötzel, Dirk Lützenkirchen−Hecht, R. Frahm, Bertram Kimmerle, Alfons Baiker, Maarten Nachtegaal, Matthias Josef Beier, Jan‐Dierk Grunwaldt

    Read original paper ↗ ·

  25. Shining X-rays on catalysts at work

    Journal of Physics Conference Series · 2009-11-01

    Jan‐Dierk Grunwaldt

    Read original paper ↗ ·

  26. Hard and soft X-ray microscopy and tomography in catalysis: bridging the different time and length scales

    Chemical Society Reviews · 2010-01-01

    Jan‐Dierk Grunwaldt, Christian G. Schroer

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  27. Hydrothermal Synthesis of Bi6S2O15 Nanowires: Structural, in situ EXAFS, and Humidity‐Sensing Studies

    Small · 2010-05-20

    Ying Zhou, Jan‐Dierk Grunwaldt, Frank Krumeich, Kaibo Zheng, Guorong Chen, Jan Stötzel, R. Frahm, Greta Ricarda Patzke

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  28. Quick-EXAFS implementation on the general purpose EXAFS beamline at ESRF

    Journal of Synchrotron Radiation · 2011-01-17

    Carmelo Prestipino, Olivier Mathon, Ricardo Hino, Antonia Beteva, S. Pascarelli

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  29. Nucleation and Aggregative Growth Process of Platinum Nanoparticles Studied by in Situ Quick XAFS Spectroscopy

    Langmuir · 2011-12-26

    Masafumi Harada, Yoshiko Kamigaito

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  30. The chemical sensitivity of X-ray spectroscopy: high energy resolution XANES versus X-ray emission spectroscopy of substituted ferrocenes

    Physical Chemistry Chemical Physics · 2013-01-01

    Andrew Atkins, Matthias Bauer, Christoph R. Jacob

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  31. QEXAFS in Catalysis Research: Principles, Data Analysis, and Applications

    Unknown journal · 2013-06-10

    Anatoly I. Frenkel, Syed Khalid, Jonathan C. Hanson, Maarten Nachtegaal

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  32. François Garin: Pioneer work in catalysis through synchrotron radiation

    Comptes Rendus Chimie · 2013-11-15

    Dominique C. Bazin

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  33. X-Ray Absorption and Scattering Methods

    Springer eBooks · 2014-01-01

    Dirk Lützenkirchen−Hecht

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  34. Cell Designs for In Situ and Operando Studies

    Springer eBooks · 2016-10-19

    Dmitry E. Doronkin, Henning Lichtenberg, Jan‐Dierk Grunwaldt

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  35. Tracking dynamic structural changes in catalysis by rapid 2D-XANES microscopy

    Journal of Synchrotron Radiation · 2021-08-12

    Saba Alizadehfanaloo, Jan Garrevoet, Martin Seyrich, Vadim Murzin, Johannes Becher, Dmitry E. Doronkin, Thomas Lennon Sheppard, Jan‐Dierk Grunwaldt, Christian G. Schroer, Andreas Schropp

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  36. Past, present and future—sample environments for materials research studies in scattering and spectroscopy; a UK perspective

    Journal of Physics Condensed Matter · 2021-09-03

    Nicholas J. Terrill, Andrew J. Dent, B. R. Dobson, Andrew Michael Beale, Lisa Allen, Wim Bras

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  37. X-Ray Microscopy and Tomography

    Springer handbooks · 2023-01-01

    Johannes Becher, Thomas Lennon Sheppard, Jan‐Dierk Grunwaldt

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  38. Operando X-ray absorption fine structure spectroscopy and its applications to catalysts

    Bulletin of the Chemical Society of Japan · 2026-03-24

    Kiyotaka Asakura

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