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RESEARCH PAPER · Journal of Nuclear Materials · 2007

Synthesis and characterization of mixed An(IV)An(III) oxalates (An(IV)=Th, Np, U or Pu and An(III)=Pu or Am)

Bénédicte Arab-Chapelet, S. Grandjean, G. Nowogrocki, F. Abraham

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Synthesis and characterization of mixed An(IV)An(III) oxalates (An(IV)=Th, Np, U or Pu and An(III)=Pu or Am)OriginalAdaptable coordination of U(IV) in the 2D-(4,4) uranium oxalate network: From 8 to 10 coordinations in the uranium (IV) oxalate hydrates74Structure of mixed U(IV)–An(III) precursors synthesized by co-conversion methods (where An=Pu, Am or Cm)72Directed Synthesis of Crystalline Plutonium(III) and (IV) Oxalates: Accessing Redox-Controlled Separations in Acidic Solutions59Transuranium Elements in the Nuclear Fuel Cycle11X-Ray Diffraction and μ-Raman Investigation of the Monoclinic-Orthorhombic Phase Transition in Th1−xUx(C2O4)2·2H2O Solid Solutions73Use of a pulsed column contactor as a continuous oxalate precipitation reactor14Stability and Structural Evolution of CeIV1–xLnIIIxO2–x/2 Solid Solutions: A Coupled μ-Raman/XRD Approach124Multiparametric Dissolution of Thorium–Cerium Dioxide Solid Solutions85Fabrication and characterization of (U, Am)O2−x transmutation targets43Synthesis and characterization of novel three-dimensional-cauliflower-like nanostructure of lead(II) oxalate and its thermal decomposition for preparation of PbO25Synthesis and characterization of Th1−xLnxO2−x/2 mixed-oxides63Single Crystal Synthesis Methods Dedicated to Structural Investigations of Very Low Solubility Mixed-Actinide Oxalate Coordination Polymers19Étude expérimentale et modélisation de la décomposition thermique d'oxalates d'actinides en oxydes0Method to Study the Primary Nucleation for Solid Solution: Application to Uranium-Neodymium Oxalate Coprecipitation5Three‐Dimensional MOF‐Type Architectures with Tetravalent Uranium Hexanuclear Motifs (U6O8)127Structural diversity of the lanthanide oxalates: Condensation of neodymium oxygen polyhedra under hydrothermal conditions7Crystal Growth and First Crystallographic Characterization of Mixed Uranium(IV)–Plutonium(III) Oxalates51Actinide oxalates, solid state structures and applications160New filterability and compressibility test cell design for nuclear products6Hydrazinium lanthanide oxalates: synthesis, structure and thermal reactivity of N2H5[Ln2(C2O4)4(N2H5)]·4H2O, Ln = Ce, Nd5Synthèse et caractérisation d'oxydes mixtes d'uranium et d'américium0Structural study of (N2H5,H)2.9U1.1Ce0.9(C2O4)5·10H2O from a conventional X-ray diffraction diagram obtained on a powder synthesized by a fast vortex process2The coprecipitation and conversion of mixed actinide oxalates for aqueous-based reprocessing of spent nuclear fuels9Low temperature decomposition of U(IV) and Th(IV) oxalates to nanograined oxide powders81A review of plutonium oxalate decomposition reactions and effects of decomposition temperature on the surface area of the plutonium dioxide product78Crystal growth methods dedicated to low solubility actinide oxalates18From uranium(IV) oxalate to sintered UO 2 : Consequences of the powders' thermal history on the microstructure41Peculiar Behavior of (U,Am)O2−δ Compounds for High Americium Contents Evidenced by XRD, XAS, and Raman Spectroscopy40Role of Ammonium Ions in the Formation of Ammonium Uranyl Peroxides and Uranyl Peroxo-oxalates20Multiscale structural characterizations of mixed U( iv )–An( iii ) oxalates (An( iii ) = Pu or Am) combining XAS and XRD measurements15UxTh1-x(C2O4)2 Solid Characterisation Studies5Melting behaviour of americium-doped uranium dioxide29The Decomposition of Oxalic Acid in Nitric Acid14Preparation, characterization and sintering of yttrium-doped ThO2 for oxygen sensors applications24Thorium aspartate tetrahydrate precursor to ThO 2 : Comparison of hydrothermal and thermal conversions27Densification behavior and microstructure evolution of yttrium-doped ThO 2 ceramics22From Nd(III) and Pu(III) Oxalates to Oxides: Influence of Nitrilotris(methylenephosphonic acid) on Chemical Composition, Structure, and Morphology9Effet de la présence de produits de fission sur les mécanismes de dissolution de composés modèles à base de dioxyde d'uranium0Synthèse et étude cristallochimique de carboxylates d'actinides tétravalents (Th, U, Np) : polymères de coordination et entités moléculaires à haute nucléarité0Molecular Assemblies of a Series of Mixed Tetravalent Uranium and Trivalent Lanthanide Complexes Associated with the Dipicolinate Ligand, in Aqueous Medium10Influence de la microstructure de la thorine yttriée sur sa tenue au sodium, en vue de réaliser des sondes à oxygène dans les réacteurs au sodium de IVème Génération.1Solid State Chemistry of Ten-Fold Coordinate Thorium(IV) Complexes with Oxalates in the Presence of Ammonium and Hydrazinium Ions9Etude de la mise en forme en forme des combustibles céramiques nucléaires par le procédé de coulage-gélification : application à l'oxyde de cérium et à des systèmes à base d'uranium0Actinide mixed oxide conversion by advanced thermal denitration route11Fabrication du combustible nucléaire par voie peroxyde : du précurseur au matériau fritté0Structural Variations of 2D and 3D Lanthanide Oxalate Frameworks Hydrothermally Synthesized in the Presence of Hydrazinium Ions13Oxidation as an Early Stage in the Multistep Thermal Decomposition of Uranium(IV) Oxalate into U 3 O 827Conversion hydrothermale d'oxalates d'actinides tétravalents : de la synthèse au frittage des poudres d'oxydes0Oxygen K-Edge X-ray Absorption Spectra of ThO2and CeO2: Experiment, Interpretation, and Structural Effects9The rapid photochemical reduction of U(VI) at high uranium concentrations relevant to spent nuclear fuel recycle processes3A review of alternative finishing options for uranium/plutonium and minor actinide nitrate products from thermal and fast reactor fuels reprocessing11238 Pu production: a State-of-the-Art review of NpO 2 target fabrication technologies and processing of irradiated targets12Chemical and spectroscopic characterization of plutonium tetrafluoride1The crystal structure of novel solid solution (UO2)0.76Th0.24(HCOO)2.46(H2O)0.760

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  1. Adaptable coordination of U(IV) in the 2D-(4,4) uranium oxalate network: From 8 to 10 coordinations in the uranium (IV) oxalate hydrates

    Journal of Solid State Chemistry · 2008-04-26

    L. Duvieubourg, Nicolas Vigier, F. Abraham, S. Grandjean

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  2. Structure of mixed U(IV)–An(III) precursors synthesized by co-conversion methods (where An=Pu, Am or Cm)

    Journal of Nuclear Materials · 2008-12-03

    S. Grandjean, Bénédicte Arab-Chapelet, Anne‐Charlotte Robisson, F. Abraham, P. Martín, J.P. Dancausse, Nathalie Herlet, Caroline Léorier

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  3. Directed Synthesis of Crystalline Plutonium(III) and (IV) Oxalates: Accessing Redox-Controlled Separations in Acidic Solutions

    Inorganic Chemistry · 2009-06-01

    Wolfgang Runde, Lia F. Brodnax, George S. Goff, Amanda C. Bean, Brian L. Scott

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  4. Transuranium Elements in the Nuclear Fuel Cycle

    Springer eBooks · 2010-01-01

    Thomas Fanghänel, J.‐P. Glatz, Rudy J. M. Konings, V.V. Rondinella, Joe Somers

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  5. X-Ray Diffraction and μ-Raman Investigation of the Monoclinic-Orthorhombic Phase Transition in Th1−xUx(C2O4)2·2H2O Solid Solutions

    Inorganic Chemistry · 2010-01-22

    Nicolas Clavier, N. Hingant, Murielle Rivenet, S. Obbade, Nicolas Dacheux, Nicole Barré, F. Abraham

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  6. Use of a pulsed column contactor as a continuous oxalate precipitation reactor

    Nuclear Engineering and Design · 2011-02-16

    Gilles Borda, Emmanuelle Brackx, Laurence Boisset, Jean Duhamet, Denis Ode

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  7. Stability and Structural Evolution of CeIV1–xLnIIIxO2–x/2 Solid Solutions: A Coupled μ-Raman/XRD Approach

    Inorganic Chemistry · 2011-06-29

    Denis Horlait, Laurent Claparède, Nicolas Clavier, Stéphanie Szenknect, Nicolas Dacheux, Johann Ravaux, Renaud Podor

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  8. Multiparametric Dissolution of Thorium–Cerium Dioxide Solid Solutions

    Inorganic Chemistry · 2011-10-25

    Laurent Claparède, Nicolas Clavier, Nicolas Dacheux, Adel Mesbah, Julien Martinez, Stéphanie Szenknect, Philippe Moisy

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  9. Fabrication and characterization of (U, Am)O2−x transmutation targets

    Journal of Nuclear Materials · 2011-12-09

    M. Vespa, Matteo Rini, José Luis Spino, Tonya Vitova, J. Somers

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  10. Synthesis and characterization of novel three-dimensional-cauliflower-like nanostructure of lead(II) oxalate and its thermal decomposition for preparation of PbO

    Inorganic Chemistry Communications · 2012-07-31

    Fatemeh Behnoudnia, Hossein Dehghani

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  11. Synthesis and characterization of Th1−xLnxO2−x/2 mixed-oxides

    Materials Research Bulletin · 2012-09-04

    Denis Horlait, Nicolas Clavier, Nicolas Dacheux, R. Cavalier, Renaud Podor

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  12. Single Crystal Synthesis Methods Dedicated to Structural Investigations of Very Low Solubility Mixed-Actinide Oxalate Coordination Polymers

    Crystal Growth & Design · 2012-09-18

    Christelle Tamain, Bénédicte Arab-Chapelet, Murielle Rivenet, F. Abraham, S. Grandjean

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  13. Étude expérimentale et modélisation de la décomposition thermique d'oxalates d'actinides en oxydes

    Unknown journal · 2012-12-19

    Lucie De almeida

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  14. Method to Study the Primary Nucleation for Solid Solution: Application to Uranium-Neodymium Oxalate Coprecipitation

    Crystal Structure Theory and Applications · 2013-01-01

    Delphine Parmentier, Murielle Bertrand, Edouard Plasari, Pascal Baron

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  15. Three‐Dimensional MOF‐Type Architectures with Tetravalent Uranium Hexanuclear Motifs (U6O8)

    Chemistry - A European Journal · 2013-01-16

    Clément Falaise, Christophe Volkringer, Jean‐François Vigier, Natacha Henry, A. Beaurain, Thierry Loiseau

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  16. Structural diversity of the lanthanide oxalates: Condensation of neodymium oxygen polyhedra under hydrothermal conditions

    Inorganic Chemistry Communications · 2013-02-21

    Alexandre Mer, Murielle Rivenet, Lucie De Almeida, S. Grandjean, F. Abraham

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  17. Crystal Growth and First Crystallographic Characterization of Mixed Uranium(IV)–Plutonium(III) Oxalates

    Inorganic Chemistry · 2013-04-11

    Christelle Tamain, Bénédicte Arab-Chapelet, Murielle Rivenet, F. Abraham, R. Caraballo, S. Grandjean

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  18. Actinide oxalates, solid state structures and applications

    Coordination Chemistry Reviews · 2013-09-06

    F. Abraham, Bénédicte Arab-Chapelet, Murielle Rivenet, Christelle Tamain, S. Grandjean

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  19. New filterability and compressibility test cell design for nuclear products

    Nuclear Engineering and Design · 2013-10-16

    J.P. Féraud, D. Bourcier, Denis Ode, François Puel

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  20. Hydrazinium lanthanide oxalates: synthesis, structure and thermal reactivity of N2H5[Ln2(C2O4)4(N2H5)]·4H2O, Ln = Ce, Nd

    Dalton Transactions · 2014-01-01

    Lucie De Almeida, S. Grandjean, Murielle Rivenet, Fabrice Patisson, F. Abraham

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  21. Synthèse et caractérisation d'oxydes mixtes d'uranium et d'américium

    Unknown journal · 2014-10-09

    Florent Lebreton

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  22. Structural study of (N2H5,H)2.9U1.1Ce0.9(C2O4)5·10H2O from a conventional X-ray diffraction diagram obtained on a powder synthesized by a fast vortex process

    Journal of Solid State Chemistry · 2014-10-21

    Emmanuelle Brackx, J.P. Laval, O. Dugne, J.P. Féraud, Bénédicte Arab-Chapelet

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  23. The coprecipitation and conversion of mixed actinide oxalates for aqueous-based reprocessing of spent nuclear fuels

    Elsevier eBooks · 2015-01-01

    Mark J. Sarsfield

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  24. Low temperature decomposition of U(IV) and Th(IV) oxalates to nanograined oxide powders

    Journal of Nuclear Materials · 2015-02-23

    Václav Tyrpekl, Jean‐François Vigier, D. Manara, T. Wiss, Oliver Dieste Blanco, Joseph Somers

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  25. A review of plutonium oxalate decomposition reactions and effects of decomposition temperature on the surface area of the plutonium dioxide product

    Journal of Nuclear Materials · 2015-07-04

    Robin M. Orr, H. Sims, Robin J. Taylor

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  26. Crystal growth methods dedicated to low solubility actinide oxalates

    Journal of Solid State Chemistry · 2015-08-01

    Christelle Tamain, Bénédicte Arab-Chapelet, Murielle Rivenet, S. Grandjean, F. Abraham

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  27. From uranium(IV) oxalate to sintered UO 2 : Consequences of the powders' thermal history on the microstructure

    Journal of the European Ceramic Society · 2015-08-29

    Julien Martinez, Nicolas Clavier, Thomas Ducasse, Adel Mesbah, Fabienne Audubert, B. Corso, Nicolas Vigier, Nicolas Dacheux

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  28. Peculiar Behavior of (U,Am)O2−δ Compounds for High Americium Contents Evidenced by XRD, XAS, and Raman Spectroscopy

    Inorganic Chemistry · 2015-09-25

    Florent Lebreton, Denis Horlait, R. Caraballo, P. Martín, Andreas C. Scheinost, A. Roßberg, Christophe Jégou, Thibaud Delahaye

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  29. Role of Ammonium Ions in the Formation of Ammonium Uranyl Peroxides and Uranyl Peroxo-oxalates

    Crystal Growth & Design · 2015-11-16

    Florent Blanchard, Marine Ellart, Murielle Rivenet, Nicolas Vigier, Isabelle Hablot, Bertrand Morel, S. Grandjean, F. Abraham

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  30. Multiscale structural characterizations of mixed U( iv )–An( iii ) oxalates (An( iii ) = Pu or Am) combining XAS and XRD measurements

    Dalton Transactions · 2016-01-01

    Bénédicte Arab-Chapelet, P. Martín, Sylvain Costenoble, Thibaud Delahaye, Andreas C. Scheinost, S. Grandjean, F. Abraham

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  31. UxTh1-x(C2O4)2 Solid Characterisation Studies

    Procedia Chemistry · 2016-01-01

    Cheryl Carrigan, Robin J. Taylor, Mark J. Sarsfield

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  32. Melting behaviour of americium-doped uranium dioxide

    The Journal of Chemical Thermodynamics · 2016-02-09

    Damien Prieur, Florent Lebreton, Marie Caisso, P. Martín, Andreas C. Scheinost, Thibaud Delahaye, D. Manara

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  33. The Decomposition of Oxalic Acid in Nitric Acid

    Journal of Solution Chemistry · 2016-02-11

    Chris Mason, T. L. Brown, D. Buchanan, Chris Maher, D. Morris, Robin J. Taylor

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  34. Preparation, characterization and sintering of yttrium-doped ThO2 for oxygen sensors applications

    Journal of Alloys and Compounds · 2016-07-30

    Marie Gabard, Yanis Hacene Cherkaski, Nicolas Clavier, L. Brissonneau, M.C. Steil, Jacques Fouletier, Adel Mesbah, Nicolas Dacheux

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  35. Thorium aspartate tetrahydrate precursor to ThO 2 : Comparison of hydrothermal and thermal conversions

    Journal of Nuclear Materials · 2017-02-23

    Nicolas Clavier, J. Maynadié, Adel Mesbah, J. Hidalgo, R. Lauwerier, G.I. Nkou Bouala, Sandra Parrès-Maynadié, Daniel J.M. Meyer, Nicolas Dacheux, Renaud Podor

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  36. Densification behavior and microstructure evolution of yttrium-doped ThO 2 ceramics

    Journal of the European Ceramic Society · 2017-04-14

    Yanis Hacene Cherkaski, Nicolas Clavier, L. Brissonneau, Renaud Podor, Nicolas Dacheux

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  37. From Nd(III) and Pu(III) Oxalates to Oxides: Influence of Nitrilotris(methylenephosphonic acid) on Chemical Composition, Structure, and Morphology

    Crystal Growth & Design · 2017-07-28

    Anne-Lise Vitart, Blaise Haidon, Bénédicte Arab-Chapelet, Murielle Rivenet, Isabelle Bisel, Patrick Pochon, Pascal Roussel, S. Grandjean, F. Abraham

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  38. Effet de la présence de produits de fission sur les mécanismes de dissolution de composés modèles à base de dioxyde d'uranium

    Unknown journal · 2017-11-27

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  39. Synthèse et étude cristallochimique de carboxylates d'actinides tétravalents (Th, U, Np) : polymères de coordination et entités moléculaires à haute nucléarité

    Unknown journal · 2017-12-07

    Nicolas P. Martin

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  40. Molecular Assemblies of a Series of Mixed Tetravalent Uranium and Trivalent Lanthanide Complexes Associated with the Dipicolinate Ligand, in Aqueous Medium

    Crystal Growth & Design · 2018-03-02

    Nicolas P. Martin, Christophe Volkringer, Natacha Henry, Sylvain Duval, Dimitrije Mara, Rik Van Deun, Thierry Loiseau

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  41. Influence de la microstructure de la thorine yttriée sur sa tenue au sodium, en vue de réaliser des sondes à oxygène dans les réacteurs au sodium de IVème Génération.

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  42. Solid State Chemistry of Ten-Fold Coordinate Thorium(IV) Complexes with Oxalates in the Presence of Ammonium and Hydrazinium Ions

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  43. Etude de la mise en forme en forme des combustibles céramiques nucléaires par le procédé de coulage-gélification : application à l'oxyde de cérium et à des systèmes à base d'uranium

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  44. Actinide mixed oxide conversion by advanced thermal denitration route

    Journal of Nuclear Materials · 2019-03-27

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  45. Fabrication du combustible nucléaire par voie peroxyde : du précurseur au matériau fritté

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  46. Structural Variations of 2D and 3D Lanthanide Oxalate Frameworks Hydrothermally Synthesized in the Presence of Hydrazinium Ions

    Inorganic Chemistry · 2019-12-24

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  47. Oxidation as an Early Stage in the Multistep Thermal Decomposition of Uranium(IV) Oxalate into U 3 O 8

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  48. Conversion hydrothermale d'oxalates d'actinides tétravalents : de la synthèse au frittage des poudres d'oxydes

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  49. Oxygen K-Edge X-ray Absorption Spectra of ThO2and CeO2: Experiment, Interpretation, and Structural Effects

    The Journal of Physical Chemistry C · 2023-02-08

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  50. The rapid photochemical reduction of U(VI) at high uranium concentrations relevant to spent nuclear fuel recycle processes

    Progress in Nuclear Energy · 2023-08-23

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