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RESEARCH PAPER · Chemical Reviews · 2010

Strategies for Solid-State NMR Studies of Materials: From Diamagnetic to Paramagnetic Porous Solids

Vladimir I. Bakhmutov

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Strategies for Solid-State NMR Studies of Materials: From Diamagnetic to Paramagnetic Porous SolidsOriginalA variable temperature solid-state nuclear magnetic resonance, electron paramagnetic resonance and Raman scattering study of molecular dynamics in ferroelectric fluorides6Acquisition of Wideline Solid-State NMR Spectra of Quadrupolar Nuclei36On Amorphous Materials as Potential Objects in Solid-State NMR Studies0Clean and Efficient Synthesis Using Mechanochemistry: Coordination Polymers, Metal-Organic Frameworks and Metallodrugs80Nonequilibrium structure of Zn2SnO4 spinel nanoparticles115Investigation of in Situ Oxalate Formation from 2,3-Pyrazinedicarboxylate under Hydrothermal Conditions Using Nuclear Magnetic Resonance Spectroscopy59Books and reviews0Solid state NMR spectroscopy2Solid-State NMR Spectroscopy of Metal–Organic Framework Compounds (MOFs)170Multinuclear solid-state NMR spectroscopy of a paramagnetic layered double hydroxide20Solid State Nuclear Magnetic Resonance of Paramagnetic Metal-Organic and -Inorganic Systems0Ethyl group as matrix modifier and inducer of ordered domains in hybrid xerogels synthesised in acidic media using ethyltriethoxysilane (ETEOS) and tetraethoxysilane (TEOS) as precursors26Computational Analysis of 47/49Ti NMR Shifts and Electric Field Gradient Tensors of Half‐Titanocene Complexes: Structure–Bonding–Property Relationships14Recent NMR developments applied to organic–inorganic materials89Solid State 13C and 2H NMR Investigations of Paramagnetic [Ni(II)(acac)2L2] Complexes15Calcium-43 chemical shift and electric field gradient tensor interplay: a sensitive probe of structure, polymorphism, and hydration26Solid‐State NMR Characterization of Paramagnetic Bis( L ‐valinato)copper(II) Stereoisomers – Effect of Conformational Disorder and Molecular Mobility on 13C and 2H Fast Magic‐Angle Spinning Spectra10Paramagnetic relaxation enhancement solid-state NMR studies of heterogeneous catalytic reaction over HY zeolite using natural abundance reactant12Water Coordination, Proton Mobility, and Lewis Acidity in HY Nanozeolites: A High-Temperature 1H and 27Al NMR Study22Couches conductrices par voie organométallique pour les dispositifs 3D en microélectronique0Solid-State NMR Study of Paramagnetic Bis(alaninato-κ2N,O)copper(II) and Bis(1-amino(cyclo)alkane-1-carboxylato-κ2N,O)copper(II) Complexes: Reflection of Stereoisomerism and Molecular Mobility in 13C and 2H Fast Magic Angle Spinning Spectra16Controlled metal nanostructures: Fertile ground for coordination chemists118Dynamic Structural Changes of SiO2 Supported Pt–Ni Bimetallic Catalysts over Redox Treatments Revealed by NMR and EPR33Atomic-level characterization of nano- and micro-structured porous materials by NMR : pushing the frontiers of sensitivity0A novel solid-state NMR method for the investigation of trivalent lanthanide sorption on amorphous silica at low surface loadings8Identification of the silver state in the framework of Ag-containing zeolite by XRD, FTIR, photoluminescence, 109 Ag NMR, EPR, DR UV-vis, TEM and XPS investigations27Structural characterization of magnesium silicate hydrate: towards the design of eco-sustainable cements125The pivotal step of nanoparticle functionalization for the preparation of functional and magnetic hybrid opal films36The Heteronuclear Multiple-Quantum Correlation Experiment: Perspective from Classical Vectors, Nonclassical Vectors, and Product Operators0Solution Layer Deposition: A Technique for the Growth of Ultra‐Pure Manganese Oxides on Silica at Room Temperature13Solution Layer Deposition: A Technique for the Growth of Ultra‐Pure Manganese Oxides on Silica at Room Temperature0Ion distribution in copper exchanged zeolites by using Si-29 spin lattice relaxation analysis431P NMR Relaxation and Motions of Phosphate Groups in Layered Zirconium Phosphate Materials15Advanced Magnetic Resonance Techniques for the Structural Characterization of Aminoxyl Radicals and Their Inorganic–Organic Nanocomposite Systems8Understanding Surface and Interfacial Chemistry in Functional Nanomaterials via Solid‐State NMR128Electrical conductivity of hydrothermally synthesized sodium lithium magnesium silicate7Nuclear Magnetic Resonance as a Tool for the Investigation of Interfaces and Textures in Nanostructured Hybrid Materials1Host-guest interaction of styrene and ethylbenzene in MIL-53 studied by solid-state NMR15Effects of dealumination on the performance of Ni-containing BEA catalysts in bioethanol steam reforming73Utilisation de méthodes avancées en RMN des solides pour la caractérisation de matériaux de type Metal-Organic Framework : étude de transformations structurales et des effets de la vapeur d’eau0Fast Magic-Angle Spinning Solid-State 1H NMR Reveals Structural Relationships in the High Explosive 2,6-Diamino-3,5-dinitropyrazine-1-oxide (LLM-105)4Photo-Uncaging of a Microtubule-Targeted Rigidin Analogue in Hypoxic Cancer Cells and in a Xenograft Mouse Model119Imprinting isolated single iron atoms onto mesoporous silica by templating with metallosurfactants31Enabling Natural Abundance 17O Solid-State NMR by Direct Polarization from Paramagnetic Metal Ions52Spatial molecular-dynamically ordered NMR spectroscopy of intact bodies and heterogeneous systems8Heterogeneous Polymer Dynamics Explored Using Static 1H NMR Spectra14Solid State NMR for Nonexperts: An Overview of Simple but General Practical Methods31Enhancing Lithium and Sodium Storage Properties of TiO2(B) Nanobelts by Doping with Nickel and Zinc31Self-assembled iron-containing mordenite monolith for carbon dioxide sieving379Monitoring electron spin fluctuations with paramagnetic relaxation enhancement17Elucidating structure and dynamics of crystalline α‐zirconium phosphates intercalated with water and methanol by multinuclear solid‐state MAS NMR: A comprehensive NMR approach8Molecular Dynamics and Surface Interactions of Nickelocene Adsorbed on Silica: A Paramagnetic Solid-State NMR Study15Miniaturization of a Nuclear Magnetic Resonance System: Architecture and Design Considerations of Transceiver Integrated Circuits17Isolated Co‐Ti‐Y Trimetallic Synergistic Catalysis Based on Apparent Anti‐Electronegative Polarization7Structure and properties of cerium phosphate and silicophosphate glasses7The Synthesis of Different Series of Cobalt BEA Zeolite Catalysts by Post-Synthesis Methods and Their Characterization11Adsorption of solid phosphines on silica and implications for catalysts on oxide surfaces4Creating Solid Solutions of Metallocenes: Migration of Nickelocene into the Ferrocene Crystal Lattice in the Absence of a Solvent8One-Shot Resin 3D-Printed Stators for Low-Cost Fabrication of Magic-Angle Spinning NMR Probeheads10Lithium‐Filled Skutterudites by Intercalation at Ambient‐Temperature2Metal ions based dynamic nuclear polarization: MI-DNP24Ex situ and in situ NMR spectroscopy and imaging for electrochemical energy storage0Understanding Cu( i ) local environments in MOFs via 63/65 Cu NMR spectroscopy12Spectroscopic Characterization of Heteroatom‐Containing Zeolites0Speciation of Lanthanide Metal Ion Dopants in Microcrystalline All-Inorganic Halide Perovskite CsPbCl332Charge transport mechanism and mechanical properties of rubidium cerium metaphosphate glasses3Paramagnetic Solid-State NMR Study of Solid Solutions of Cobaltocene with Ferrocene and Nickelocene3NMR of Organic Linkers in MOFs and COFs2State-of-the-Art ASIC for Micro-NMR Transceiver: Architecture and Design Considerations0The role of spin diffusion in endogenous metal ions DNP435Cl NMR of Metal‐Organic Frameworks: What Can We Learn?4A Comprehensive Solution and Solid-State NMR Study of Proton Spin Lattice Relaxation in Paramagnetic Metallocenes1TEMPO in Solution, Melted, Solid, and Adsorbed on a Silica Surface: A Paramagnetic NMR Study1Engineering Paramagnetic Spin Centers in Metal-Free Organic Frameworks1Accessing High-Nuclearity Cluster-Based Metal−Organic Frameworks Using Early Lanthanoids: A Study of RE-UiO-660Surfactants as molecular architects of materials: from interfacial organization to function1The use of solid state NMR to monitor reactions and doping in inorganic materials0

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  4. Clean and Efficient Synthesis Using Mechanochemistry: Coordination Polymers, Metal-Organic Frameworks and Metallodrugs

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  6. Investigation of in Situ Oxalate Formation from 2,3-Pyrazinedicarboxylate under Hydrothermal Conditions Using Nuclear Magnetic Resonance Spectroscopy

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