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RESEARCH PAPER · Chemical Reviews · 2012

Recent Advances in the Synthesis and Application of Layered Double Hydroxide (LDH) Nanosheets

Qiang Wang, Dermot M. O'Hare

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Recent Advances in the Synthesis and Application of Layered Double Hydroxide (LDH) NanosheetsOriginalLayered α‐Co(OH)2 Nanocones as Electrode Materials for Pseudocapacitors: Understanding the Effect of Interlayer Space on Electrochemical Activity311Enhanced low-temperature activity of CO2 methanation over highly-dispersed Ni/TiO2 catalyst308Layered double hydroxide-based catalysts: nanostructure design and catalytic performance333LDH nanocages synthesized with MOF templates and their high performance as supercapacitors665Graphene-Like Two-Dimensional Materials4531Calcined graphene/MgAl-layered double hydroxides for enhanced Cr(VI) removal350Solvothermal One-Step Synthesis of Ni–Al Layered Double Hydroxide/Carbon Nanotube/Reduced Graphene Oxide Sheet Ternary Nanocomposite with Ultrahigh Capacitance for Supercapacitors272Pearson’s Principle Inspired Generalized Strategy for the Fabrication of Metal Hydroxide and Oxide Nanocages314Hierarchical Nanowire Arrays Based on ZnO Core−Layered Double Hydroxide Shell for Largely Enhanced Photoelectrochemical Water Splitting276Recent advances on polyoxometalates intercalated layered double hydroxides: From synthetic approaches to functional material applications283Nickel–Cobalt Layered Double Hydroxide Nanosheets for High‐performance Supercapacitor Electrode Materials1419NiTi-Layered double hydroxides nanosheets as efficient photocatalysts for oxygen evolution from water using visible light279A sandwich-type three-dimensional layered double hydroxide nanosheet array/graphene composite: fabrication and high supercapacitor performance289Flame retardant polymer/layered double hydroxide nanocomposites351Three-dimensional NiFe layered double hydroxide film for high-efficiency oxygen evolution reaction894Ultrafast high-capacity NiZn battery with NiAlCo-layered double hydroxide309Intercalation of drugs in layered double hydroxides and their controlled release: A review403Hierarchical NiMn Layered Double Hydroxide/Carbon Nanotubes Architecture with Superb Energy Density for Flexible Supercapacitors747Nitrogen‐Doped Graphene/Carbon Nanotube Hybrids: In Situ Formation on Bifunctional Catalysts and Their Superior Electrocatalytic Activity for Oxygen Evolution/Reduction Reaction614Unstacked double-layer templated graphene for high-rate lithium–sulphur batteries664Catalytic applications of layered double hydroxides: recent advances and perspectives1762Layered Double Hydroxide‐based Nanomaterials as Highly Efficient Catalysts and Adsorbents451A mini review of NiFe-based materials as highly active oxygen evolution reaction electrocatalysts1440Two-Dimensional Oxide and Hydroxide Nanosheets: Controllable High-Quality Exfoliation, Molecular Assembly, and Exploration of Functionality523Hierarchical layered double hydroxide nanocomposites: structure, synthesis and applications389Two-dimensional graphene analogues for biomedical applications898Fast electrosynthesis of Fe-containing layered double hydroxide arrays toward highly efficient electrocatalytic oxidation reactions443Layered double hydroxides toward electrochemical energy storage and conversion: design, synthesis and applications451Visible light-driven novel g-C 3 N 4 /NiFe-LDH composite photocatalyst with enhanced photocatalytic activity towards water oxidation and reduction reaction613One‐Pot, Facile, and Versatile Synthesis of Monolayer MoS 2 /WS 2 Quantum Dots as Bioimaging Probes and Efficient Electrocatalysts for Hydrogen Evolution Reaction826Solvothermal synthesis of NiCo-layered double hydroxide nanosheets decorated on RGO sheets for high performance supercapacitor522A review on coke management during dry reforming of methane381Hydrothermal Continuous Flow Synthesis and Exfoliation of NiCo Layered Double Hydroxide Nanosheets for Enhanced Oxygen Evolution Catalysis983Trinary Layered Double Hydroxides as High‐Performance Bifunctional Materials for Oxygen Electrocatalysis387Porous Two-Dimensional Nanosheets Converted from Layered Double Hydroxides and Their Applications in Electrocatalytic Water Splitting298Pd–Co based spinel oxides derived from pd nanoparticles immobilized on layered double hydroxides for toluene combustion265Wet-chemical synthesis and applications of non-layer structured two-dimensional nanomaterials651Ultrathin Two-Dimensional Nanomaterials2167Transition metal based layered double hydroxides tailored for energy conversion and storage572Defect‐Rich Ultrathin ZnAl‐Layered Double Hydroxide Nanosheets for Efficient Photoreduction of CO2 to CO with Water766Ternary NiFeMn layered double hydroxides as highly-efficient oxygen evolution catalysts345Layered Double Hydroxide Nanostructured Photocatalysts for Renewable Energy Production484Sulfidation of NiMn‐Layered Double Hydroxides/Graphene Oxide Composites toward Supercapacitor Electrodes with Enhanced Performance292Ultrathin nanoflakes of cobalt–manganese layered double hydroxide with high reversibility for asymmetric supercapacitor318Rational designs and engineering of hollow micro-/nanostructures as sulfur hosts for advanced lithium–sulfur batteries654Ultrathin two-dimensional layered metal hydroxides: an emerging platform for advanced catalysis, energy conversion and storage451Nanoencapsulation, Nano-guard for Pesticides: A New Window for Safe Application975A flexible all-solid-state micro-supercapacitor based on hierarchical CuO@layered double hydroxide core–shell nanoarrays342Large Scale Synthesis of NiCo Layered Double Hydroxides for Superior Asymmetric Electrochemical Capacitor289Directed Growth of Metal‐Organic Frameworks and Their Derived Carbon‐Based Network for Efficient Electrocatalytic Oxygen Reduction498Double‐Shelled Nanocages with Cobalt Hydroxide Inner Shell and Layered Double Hydroxides Outer Shell as High‐Efficiency Polysulfide Mediator for Lithium–Sulfur Batteries560Ni3FeN Nanoparticles Derived from Ultrathin NiFe‐Layered Double Hydroxide Nanosheets: An Efficient Overall Water Splitting Electrocatalyst772Hierarchical Core–Shell Al 2 O 3 @Pd-CoAlO Microspheres for Low-Temperature Toluene Combustion355Biomedical Uses for 2D Materials Beyond Graphene: Current Advances and Challenges Ahead417The growth of nickel-manganese and cobalt-manganese layered double hydroxides on reduced graphene oxide for supercapacitor304Ultrafine NiO Nanosheets Stabilized by TiO 2 from Monolayer NiTi-LDH Precursors: An Active Water Oxidation Electrocatalyst730Cotton-textile-enabled flexible self-sustaining power packs via roll-to-roll fabrication331Nanoparticle-Stacked Porous Nickel–Iron Nitride Nanosheet: A Highly Efficient Bifunctional Electrocatalyst for Overall Water Splitting315Two‐Dimensional‐Material Membranes: A New Family of High‐Performance Separation Membranes841Van der Waals heterostructures and devices2793Phosphorene and Phosphorene‐Based Materials – Prospects for Future Applications494Two‐Dimensional Metal Oxide and Metal Hydroxide Nanosheets: Synthesis, Controlled Assembly and Applications in Energy Conversion and Storage277Few‐Layer Antimonene by Liquid‐Phase Exfoliation415Transition‐Metal (Co, Ni, and Fe)‐Based Electrocatalysts for the Water Oxidation Reaction1769Recent Advances in Heterogeneous Photocatalytic CO 2 Conversion to Solar Fuels1350Hierarchical CoNi‐Sulfide Nanosheet Arrays Derived from Layered Double Hydroxides toward Efficient Hydrazine Electrooxidation264A hierarchical CoFe-layered double hydroxide modified carbon-felt cathode for heterogeneous electro-Fenton process320Deep eutectic solvents (DESs)-derived advanced functional materials for energy and environmental applications: challenges, opportunities, and future vision370Preparation of two dimensional layered double hydroxide nanosheets and their applications924Nanoparticle decoration with surfactants: Molecular interactions, assembly, and applications608Two-Dimensional (2D) Nanomaterials towards Electrochemical Nanoarchitectonics in Energy-Related Applications432Amorphous Cobalt–Iron Hydroxide Nanosheet Electrocatalyst for Efficient Electrochemical and Photo‐Electrochemical Oxygen Evolution357Recent Advances in Ultrathin Two-Dimensional Nanomaterials5100Two‐Dimensional Metal Oxide Nanomaterials for Next‐Generation Rechargeable Batteries4592-Methylimidazole-Derived Ni–Co Layered Double Hydroxide Nanosheets as High Rate Capability and High Energy Density Storage Material in Hybrid Supercapacitors459In Situ Transformation of MOFs into Layered Double Hydroxide Embedded Metal Sulfides for Improved Electrocatalytic and Supercapacitive Performance643Oxidation Stability of Colloidal Two-Dimensional Titanium Carbides (MXenes)1725Synthesis of Ultrathin PdCu Alloy Nanosheets Used as a Highly Efficient Electrocatalyst for Formic Acid Oxidation292Development Strategies and Prospects of Nano-based Smart Pesticide Formulation698CO 2 Reduction: From the Electrochemical to Photochemical Approach937First‐Row Transition Metal Based Catalysts for the Oxygen Evolution Reaction under Alkaline Conditions: Basic Principles and Recent Advances500Layered‐Double‐Hydroxide Nanosheets as Efficient Visible‐Light‐Driven Photocatalysts for Dinitrogen Fixation706Recent advance in MXenes: A promising 2D material for catalysis, sensor and chemical adsorption659Recent Progress on Antimonene: A New Bidimensional Material300Electronic Structure Reconfiguration toward Pyrite NiS2 via Engineered Heteroatom Defect Boosting Overall Water Splitting385Tailoring Hybrid Layered Double Hydroxides for the Development of Innovative Applications320Hierarchical FeCo2O4@NiCo layered double hydroxide core/shell nanowires for high performance flexible all-solid-state asymmetric supercapacitors450Alumina‐Supported CoFe Alloy Catalysts Derived from Layered‐Double‐Hydroxide Nanosheets for Efficient Photothermal CO2 Hydrogenation to Hydrocarbons469Catalysis of Carbon Dioxide Photoreduction on Nanosheets: Fundamentals and Challenges480g-C 3 N 4 /NiAl-LDH 2D/2D Hybrid Heterojunction for High-Performance Photocatalytic Reduction of CO 2 into Renewable Fuels556Conductive two-dimensional metal–organic frameworks as multifunctional materials530Preparation of 2D material dispersions and their applications665Two-dimensional metal–organic framework nanosheets: synthesis and applications1348Accelerated Hydrogen Evolution Kinetics on NiFe‐Layered Double Hydroxide Electrocatalysts by Tailoring Water Dissociation Active Sites934Tuning Electronic Structure of NiFe Layered Double Hydroxides with Vanadium Doping toward High Efficient Electrocatalytic Water Oxidation757Sub‐3 nm Ultrafine Monolayer Layered Double Hydroxide Nanosheets for Electrochemical Water Oxidation339Introducing Fe 2+ into Nickel–Iron Layered Double Hydroxide: Local Structure Modulated Water Oxidation Activity398Interface-Assisted Synthesis of 2D Materials: Trend and Challenges710Two-Dimensional Metal Nanomaterials: Synthesis, Properties, and Applications999Corrosion engineering towards efficient oxygen evolution electrodes with stable catalytic activity for over 6000 hours563Recent Progress on Nickel‐Based Oxide/(Oxy)Hydroxide Electrocatalysts for the Oxygen Evolution Reaction268Synthesis of amorphous nickel–cobalt–manganese hydroxides for supercapacitor-battery hybrid energy storage system303Two-Dimensional MXene (Ti3C2)-Integrated Cellulose Hydrogels: Toward Smart Three-Dimensional Network Nanoplatforms Exhibiting Light-Induced Swelling and Bimodal Photothermal/Chemotherapy Anticancer Activity488Layered Double Hydroxide‐Based Catalysts: Recent Advances in Preparation, Structure, and Applications605Layered and two dimensional metal oxides for electrochemical energy conversion396A review on effect of synthesis conditions on the formation of layered double hydroxides414Two-dimensional-related catalytic materials for solar-driven conversion of CO x into valuable chemical feedstocks435Heterostructures Based on 2D Materials: A Versatile Platform for Efficient Catalysis264Recent advances in layered double hydroxide electrocatalysts for the oxygen evolution reaction6042D Black Phosphorus–Based Biomedical Applications583Enhancing Electrocatalytic Water Splitting by Strain Engineering787A review on strategies to LDH-based materials to improve adsorption capacity and photoreduction efficiency for CO22892D Layered Double Hydroxides for Oxygen Evolution Reaction: From Fundamental Design to Application730NiCoMo Hydroxide Nanosheet Arrays Synthesized via Chloride Corrosion for Overall Water Splitting307Multicomponent Hierarchical Cu‐Doped NiCo‐LDH/CuO Double Arrays for Ultralong‐Life Hybrid Fiber Supercapacitor468A review on the recent advances, challenges and future aspect of layered double hydroxides (LDH) – Containing hybrids as promising adsorbents for dyes removal300Atomic and electronic modulation of self-supported nickel-vanadium layered double hydroxide to accelerate water splitting kinetics557A highly alkaline-stable metal oxide@metal–organic framework composite for high-performance electrochemical energy storage620Two-dimensional nanomaterials: fascinating materials in biomedical field309Functionalized layered double hydroxides for innovative applications314Two-dimensional photocatalyst design: A critical review of recent experimental and computational advances416Industrial carbon dioxide capture and utilization: state of the art and future challenges1383Self-assembly of block copolymers towards mesoporous materials for energy storage and conversion systems513Activating the hydrogen evolution and overall water splitting performance of NiFe LDH by cation doping and plasma reduction453Efficient Photocatalytic Nitrogen Fixation over Cu δ + ‐Modified Defective ZnAl‐Layered Double Hydroxide Nanosheets284The roles and mechanism of cocatalysts in photocatalytic water splitting to produce hydrogen274Transition metal based battery-type electrodes in hybrid supercapacitors: A review710High-Flux Vertically Aligned 2D Covalent Organic Framework Membrane with Enhanced Hydrogen Separation350Cr-doped CoFe layered double hydroxides: Highly efficient and robust bifunctional electrocatalyst for the oxidation of water and urea340Positioning MXenes in the Photocatalysis Landscape: Competitiveness, Challenges, and Future Perspectives276Alkali Etching of Layered Double Hydroxide Nanosheets for Enhanced Photocatalytic N2 Reduction to NH3271Chemical Modifications of Layered Double Hydroxides in the Supercapacitor280State of the art recent progress in two dimensional MXenes based gas sensors and biosensors: A comprehensive review282Sustainable wastewater treatment by biochar/layered double hydroxide composites: Progress, challenges, and outlook302Recent advances in magnesium/lithium separation and lithium extraction technologies from salt lake brine681Topotactically Transformed Polygonal Mesopores on Ternary Layered Double Hydroxides Exposing Under‐Coordinated Metal Centers for Accelerated Water Dissociation324Recent advances in highly active nanostructured NiFe LDH catalyst for electrochemical water splitting463Deciphering the alternating synergy between interlayer Pt single-atom and NiFe layered double hydroxide for overall water splitting587Layered double hydroxide-based electrocatalysts for the oxygen evolution reaction: identification and tailoring of active sites, and superaerophobic nanoarray electrode assembly761Two-dimensional biomaterials: material science, biological effect and biomedical engineering applications285Artificial channels for confined mass transport at the sub-nanometre scale526Intercalation as a versatile tool for fabrication, property tuning, and phase transitions in 2D materials268A review of material aspects in developing direct Z-scheme photocatalysts388Layered double hydroxide (LDH)-based materials: A mini-review on strategies to improve the performance for photocatalytic water splitting314NiCo-Based Electrocatalysts for the Alkaline Oxygen Evolution Reaction: A Review433Interfacial Assembly and Applications of Functional Mesoporous Materials368Layered double hydroxide-based nanomaterials for biomedical applications440A review of Ni based powder catalyst for urea oxidation in assisting water splitting reaction271Insights into 2D/2D MXene Heterostructures for Improved Synergy in Structure toward Next‐Generation Supercapacitors: A Review439Oxygen Evolution/Reduction Reaction Catalysts: From In Situ Monitoring and Reaction Mechanisms to Rational Design802

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