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RESEARCH PAPER · Chemistry of Materials · 2005

Three-Dimensionally Ordered Macroporous Li4Ti5O12: Effect of Wall Structure on Electrochemical Properties

Erin M. Sorensen, Scott J. Barry, Ha‐Kyun Jung, James M. Rondinelli, John T. Vaughey, Kenneth Reinhard Poeppelmeier

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Three-Dimensionally Ordered Macroporous Li4Ti5O12: Effect of Wall Structure on Electrochemical PropertiesOriginalPhotonic Crystal Structures as a Basis for a Three‐Dimensionally Interpenetrating Electrochemical‐Cell System106The Role of Thickness Transitions in Convective Assembly84A study of nitroxide polyradical/activated carbon composite as the positive electrode material for electrochemical hybrid capacitor39Hierarchically Porous Rutile Titania: Harnessing Spontaneous Compositional Change in Mixed-Metal Oxides32Quantifying stacking faults and vacancies in thin convectively assembled colloidal crystals20Fabrication of a Fully Infiltrated Three-Dimensional Solid-State Interpenetrating Electrochemical Cell58Spinel Li[sub 4]Ti[sub 5]O[sub 12] Nanowires for High-Rate Li-Ion Intercalation Electrode138Nanoporous cuprous oxide/lithia composite anode with capacity increasing characteristic and high rate capability76Preparation and rate capability of Li4Ti5O12 hollow-sphere anode material125An infrared study of the surface chemistry of lithium titanate spinel (Li4Ti5O12)43The role of fluid flow and convective steering during the assembly of colloidal crystals36Microwave solid-state synthesis of spinel Li4Ti5O12 nanocrystallites as anode material for lithium-ion batteries149Role of Electrochemically Driven Cu Nanograins in CuGa2 Electrode29Morphological Control in Colloidal Crystal Templating of Inverse Opals, Hierarchical Structures, and Shaped Particles488Template-Directed Materials for Rechargeable Lithium-Ion Batteries539Porous Carbon/Tin (IV) Oxide Monoliths as Anodes for Lithium-Ion Batteries51The Synthesis of Hollow Spherical Li[sub 4]Ti[sub 5]O[sub 12] by Macroemulsion Method and its Application in Li-Ion Batteries23Synthesis, structure, and electrochemical Li-ion intercalation properties of Li2Ti3O7 with Na2Ti3O7-type layered structure73Uniform Polystyrene Particles by Dispersion Polymerization in Different Dispersion Medium24Fast and reversible lithium-induced electrochemical alloying in tin-based composite oxide hierarchical microspheres assembled by nanoplate building blocks9Influence of high-energy ball milling of precursor on the morphology and electrochemical performance of Li4Ti5O12–ball-milling time48Three-Dimensionally Ordered Macroporous Lithium Manganese Oxide for Rechargeable Lithium Batteries89Polyaniline nanofibers as the electrode material for supercapacitors175Synthesis of monolithic 3D ordered macroporous carbon/nano-silicon composites by diiodosilane decomposition36Preparation and electrochemical lithium storage of flower-like spinel Li4Ti5O12 consisting of nanosheets180Characteristics of spherical-shaped Li4Ti5O12 anode powders prepared by spray pyrolysis43Combustion synthesis of high-performance Li4Ti5O12 for secondary Li-ion battery132A simple gel route to synthesize nano-Li4Ti5O12 as a high-performance anode material for Li-ion batteries58Synthesis and electrochemical performance of nano-sized Li4Ti5O12 with double surface modification of Ti(III) and carbon250Template-free synthesis of mesoporous spinel lithium titanate microspheres and their application in high-rate lithium ion batteries134Improving electrochemical performance of NiO films by electrodeposition on foam nickel substrates54Electrochemical and structural characterization of lithium titanate electrodes19Study on the Theoretical Capacity of Spinel Lithium Titanate Induced by Low-Potential Intercalation176Preparation and electrochemical properties of Li4Ti5O12 thin film electrodes by pulsed laser deposition58Synthesis of spinel Li4Ti5O12 anode material by a modified rheological phase reaction76Silicon Inverse‐Opal‐Based Macroporous Materials as Negative Electrodes for Lithium Ion Batteries271HEBM synthesis of nanocrystalline LiZn0.5Ti1.5O4 spinel and thermally induced order–disorder phase transition16Li4Ti5O12 hollow microspheres assembled by nanosheets as an anode material for high-rate lithium ion batteries165Spinel Li4Ti5O12 Nanotubes for Energy Storage Materials120Synthesis and electrochemical evaluation of an amorphous titanium dioxide derived from a solid state precursor15General synthesis of carbon-coated nanostructure Li 4 Ti 5 O 12 as a high rate electrode material for Li-ion intercalation257Synthesis of lithium insertion material Li4Ti5O12 from rutile TiO2 via surface activation49Improvement of the high rate capability of hierarchical structured Li4Ti5O12 induced by the pseudocapacitive effect142Facile synthesis of hierarchically porous Li4Ti5O12 microspheres for high rate lithium ion batteries275MnO/C Nanocomposites as High Capacity Anode Materials for Li-Ion Batteries82Ordered multimodal porous carbon with hierarchical nanostructure for high Li storage capacity and good cycling performance124Facile synthesis and high rate capability of Li4Ti5O12/C composite materials with controllable carbon content25Basic molten salt process—A new route for synthesis of nanocrystalline Li4Ti5O12–TiO2 anode material for Li-ion batteries using eutectic mixture of LiNO3–LiOH–Li2O296High capacity three-dimensional ordered macroporous CoFe2O4 as anode material for lithium ion batteries203Solution-Combustion Synthesized Nanocrystalline Li4Ti5O12 As High-Rate Performance Li-Ion Battery Anode422Recent development and application of Li4Ti5O12 as anode material of lithium ion battery372Preparation and re-examination of Li4Ti4.85Al0.15O12 as anode material of lithium-ion battery35Influence of Li addition on charge/discharge behavior of spinel lithium titanate28Ordered Porous Crystalline Transition Metal Oxides5In situ growth of Li 4 Ti 5 O 12 on multi-walled carbon nanotubes: novel coaxial nanocables for high rate lithium ion batteries187In situ synthesis of high-loading Li 4 Ti 5 O 12 –graphene hybrid nanostructures for high rate lithium ion batteries187Surfactant-free nonaqueous synthesis of lithium titanium oxide (LTO) nanostructures for lithium ion battery applications85Roles of nanosize in lithium reactive nanomaterials for lithium ion batteries415Carbon-coated nano-sized Li4Ti5O12 nanoporous micro-sphere as anode material for high-rate lithium-ion batteries390Electrochemical intercalation of Mg2+ in 3D hierarchically porous magnesium cobalt silicate and its application as an advanced cathode material in rechargeable magnesium batteries59Enhanced High-Rate Performance of Li[sub 4]Ti[sub 5]O[sub 12] Nanoparticles for Rechargeable Li-Ion Batteries82Natural products targeting telomere maintenance41Ultra-high Li storage capacity achieved by hollow carbon capsules with hierarchical nanoarchitecture75Novel Li4Ti5O12/Sn nano-composites as anode material for lithium ion batteries61Amorphous Carbon Coated High Grain Boundary Density Dual Phase Li4Ti5O12‐TiO2: A Nanocomposite Anode Material for Li‐Ion Batteries302P123-PMMA Dual-Templating Generation and Unique Physicochemical Properties of Three-Dimensionally Ordered Macroporous Iron Oxides with Nanovoids in the Crystalline Walls86Effect of Heat-treatment Temperature on the Structure and Properties of Li4Ti5O12 Nanorods Prepared by the Hydrothermal Ion Exchange Method3Cage-Shape Macroporous/Mesoporous 3DOM SiO2 Immobilized Papain2Preparation and characterization of macroporous LiNi1/3Co1/3Mn1/3O2 using carbon sphere as template32Surfactant-mediated PMMA-templating fabrication and characterization of three-dimensionally ordered macroporous Eu2O3 and Sm2O3 with mesoporous walls41Preparation of Li4Ti5O12 submicrospheres and their application as anode materials of rechargeable lithium-ion batteries17Nanosized Li4Ti5O12/graphene hybrid materials with low polarization for high rate lithium ion batteries322Rapid Synthesis of Li4Ti5O12 Microspheres as Anode Materials and Its Binder Effect for Lithium-Ion Battery396High rate capability and long-term cyclability of Li4Ti4.9V0.1O12 as anode material in lithium ion battery110Synthesis of spinel lithium titanate anodes incorporated with rutile titania nanocrystallites by spray drying followed by calcination33Low‐temperature Synthesis of Peony‐like Spinel Li4Ti5O12 as a High‐performance Anode Material for Lithium Ion Batteries6Highly Improved Rate Capability for a Lithium‐Ion Battery Nano‐Li4Ti5O12 Negative Electrode via Carbon‐Coated Mesoporous Uniform Pores with a Simple Self‐Assembly Method277Improved rate capability of carbon coated Li3.9Sn0.1Ti5O12 porous electrodes for Li-ion batteries97Facile synthesis of mesoporous lithium titanate spheres for high rate lithium-ion batteries72Phenol–formaldehyde resin-assisted synthesis of pure porous Li4Ti5O12 for rate capability improvement10Improvement of rate capability of spinel lithium titanate anodes using microwave-assisted zinc nanocoating38Preparation of a spinel Li4Ti5O12 (111) surface from a rutile TiO2 single crystal28Enhancing the performances of Li-ion batteries by carbon-coating: present and future967Li4Ti5O12 nanocrystallites for high-rate lithium-ion batteries synthesized by a rapid microwave-assisted solid-state process61A novel grain restraint strategy to synthesize highly crystallized Li4Ti5O12 (∼20 nm) for lithium ion batteries with superior high-rate performance49Inverse Opal Nanoarchitectures as Lithium-Ion Battery Materials0Large-scale selective preparation of porous SnO2 3D architectures and their gas-sensing property57Nitrogen- and TiN-modified Li4Ti5O12: one-step synthesis and electrochemical performance optimization113Preparation and Characterization of Porous Spherical Li4Ti5O12/C Anode Material for Lithium Ion Batteries0Structure Characterization and Electrochemical Characteristics of Carbon Nanotube- Spinel Li4Ti5O12Nanoparticles0Superior high rate performance of core–shell Li4Ti5O12/carbon nanocomposite synthesized by a supercritical alcohol approach49Ti-based compounds as anode materials for Li-ion batteries863Urchin-like Li4Ti5O12–carbon nanofiber composites for high rate performance anodes in Li-ion batteries138Magnesium cobalt silicate materials for reversible magnesium ion storage93Film-shaped sol–gel Li4Ti5O12 electrode for lithium-ion microbatteries44Preparation and Characteristics of Li4Ti5O12Anode Material for Hybrid Supercapacitor31Nanostructured Li4Ti5O12 synthesized in a reverse micelle: A bridge between pseudocapacitor and lithium ion battery16Defective mesoporous Li4Ti5O12−y: An advanced anode material with anomalous capacity and cycling stability at a high rate of 20C58Improving electrochemical properties of spinel lithium titanate by incorporation of titanium nitride via high-energy ball-milling37Rutile-TiO2 Nanocoating for a High-Rate Li4Ti5O12 Anode of a Lithium-Ion Battery629Nano-Li4Ti5O12 anchored on carbon nanotubes by liquid phase deposition as anode material for high rate lithium-ion batteries93Self-assembled synthesis of nanoflower-like Li4Ti5O12 for ultrahigh rate lithium-ion batteries62Three-Dimensional Coherent Titania–Mesoporous Carbon Nanocomposite and Its Lithium-Ion Storage Properties89Synthesis of Li4Ti5O12 in supercritical water for Li-ion batteries: Reaction mechanism and high-rate performance43Hierarchically Structured Porous Materials for Energy Conversion and Storage953Facile synthesis of nanocrystalline Li4Ti5O12 by microemulsion and its application as anode material for Li-ion batteries49Self-assembled synthesis of monodispersed mesoporous Li4Ti5O12 beads and their applications in secondary lithium-ion batteries15Electrochemical profile of lithium titanate/hard carbon composite as anode material for Li-ion batteries25Porous Electrode Materials for Lithium‐Ion Batteries – How to Prepare Them and What Makes Them Special725A high energy and power density hybrid supercapacitor based on an advanced carbon-coated Li4Ti5O12 electrode200Synthesis, characterization and electrochemical properties of three-dimensionally ordered macroporous α-Fe2O310Binary Li4Ti5O12‐Li2Ti3O7 Nanocomposite as an Anode Material for Li‐Ion Batteries94Synthesis and electrochemical performance of high-rate dual-phase Li4Ti5O12–TiO2 nanocrystallines for Li-ion batteries63Design and functionality of colloidal-crystal-templated materials—chemical applications of inverse opals555Ru-doped Li4Ti5O12 anode materials for high rate lithium-ion batteries70Solid lithium electrolyte-Li4Ti5O12 composites as anodes of lithium-ion batteries showing high-rate performance30Acid-assisted synthesis of dandelion-like rutile TiO2 and Li4Ti5O12 mesoporous spheres: towards an efficient lithium battery application10Comparison of Structural Analysis and Electrochemical Studies of C-Li4Ti5O12and CNT-Li4Ti5O12Nanocomposites particles used as Anode for Lithium Ion Battery0New Li2FeSiO4–carbon monoliths with controlled macropores: effects of pore properties on electrode performance18SBA-15 confined synthesis of TiNb2O7 nanoparticles for lithium-ion batteries134The Characterization of Lithium Titanate Microspheres Synthesized by a Hydrothermal Method16Evaluation of Pulsed Laser Deposited Li4Ti5O12 Thin Film Anodes by CV and EIS5Ultrathin atomic layer deposited ZrO2 coating to enhance the electrochemical performance of Li4Ti5O12 as an anode material106Nano-Li4Ti5O12 Pore Microspheres: A High Power Electrode Material for Lithium Ion Batteries16Facile preparation of Li4Ti5O12/AB/MWCNTs composite with high-rate performance for lithium ion battery24Mesoporous Li4Ti5O12 Hollow Spheres with Enhanced Lithium Storage Capability375Simply AlF3-treated Li4Ti5O12 composite anode materials for stable and ultrahigh power lithium-ion batteries51Biomass pyrolysis/gasification using three dimensional ordered macroporous (3DOM) Fe2O3 as an oxygen carrier3Electrochemical Properties of Nano-sized Li4Ti5O12 Powders Prepared by Flame Spray Pyrolysis11Facile synthesis of hierarchical mesoporous Li4Ti5O12 microspheres in supercritical methanol42Ultrathin Atomic Layer Deposited ZrO2 Coating to Enhance the Electrochemical Performance of Li4Ti5O12 as an Anode Material2Effects of a dopant on the electrochemical properties of Li4Ti5O12 as a lithium-ion battery anode material41Li4Ti5O12 Nanocrystals Synthesized by Carbon Templating from Solution Precursors Yield High Performance Thin Film Li‐Ion Battery Electrodes77Structural characterization and electrochemical behaviour of Li(4−x)/3Ti(5−2x)/3MnxO4 solid solution with spinel-structure4Synthesis and electrochemical characterisation of electrospun lithium titanate ultrafine fibres20Surface nitridation induced high electrochemical performance of Li4Ti5O12 using urea as a nitrogen source18Synthesis and characterization of silver/lithium cobalt oxide (Ag/LiCoO2) nanofibers via sol–gel electrospinning23Graphene-based Li-ion hybrid supercapacitors with ultrahigh performance219Oxides for Li Intercalation, Li‐ion Batteries0Carbon inverse opal entrapped with electrode active nanoparticles as high-performance anode for lithium-ion batteries86Synthesis and electrochemical performance of F-doped Li4Ti5O12 for lithium-ion batteries86Oxides for Li Intercalation, Li‐ion Batteries0Nanostructured lithium titanate and lithium titanate/carbon nanocomposite as anode materials for advanced lithium-ion batteries28Templated spinel Li4Ti5O12 Li-ion battery electrodes combining high rates with high energy density25Hierarchically structured materials for lithium batteries32Nanostructures in Electrochromic Materials3Impact des phénomènes aux interfaces électrode/électrolyte sur les performances des batteries Li-ion haute tension : faiblesses et atouts des électrolytes à base de carbonates d'alkyles et de sulfones face aux électrodes LiNi0,4Mn1,6 O4 et Li4Ti5O120Electrochemical and thermal characterization of lithium titanate spinel anode in C–LiFePO4//C–Li4Ti5O12 cells at sub-zero temperatures56A nanoparticle Mg-doped Li4Ti5O12 for high rate lithium-ion batteries108One-Pot Facile Synthesis of Ant-Cave-Structured Metal Oxide–Carbon Microballs by Continuous Process for Use as Anode Materials in Li-Ion Batteries159

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  1. Photonic Crystal Structures as a Basis for a Three‐Dimensionally Interpenetrating Electrochemical‐Cell System

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  8. Nanoporous cuprous oxide/lithia composite anode with capacity increasing characteristic and high rate capability

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  9. Preparation and rate capability of Li4Ti5O12 hollow-sphere anode material

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  10. An infrared study of the surface chemistry of lithium titanate spinel (Li4Ti5O12)

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  13. Role of Electrochemically Driven Cu Nanograins in CuGa2 Electrode

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  14. Morphological Control in Colloidal Crystal Templating of Inverse Opals, Hierarchical Structures, and Shaped Particles

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  18. Synthesis, structure, and electrochemical Li-ion intercalation properties of Li2Ti3O7 with Na2Ti3O7-type layered structure

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  21. Influence of high-energy ball milling of precursor on the morphology and electrochemical performance of Li4Ti5O12–ball-milling time

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  22. Three-Dimensionally Ordered Macroporous Lithium Manganese Oxide for Rechargeable Lithium Batteries

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  26. Characteristics of spherical-shaped Li4Ti5O12 anode powders prepared by spray pyrolysis

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  38. Li4Ti5O12 hollow microspheres assembled by nanosheets as an anode material for high-rate lithium ion batteries

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  39. Spinel Li4Ti5O12 Nanotubes for Energy Storage Materials

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  40. Synthesis and electrochemical evaluation of an amorphous titanium dioxide derived from a solid state precursor

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  41. General synthesis of carbon-coated nanostructure Li 4 Ti 5 O 12 as a high rate electrode material for Li-ion intercalation

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  42. Synthesis of lithium insertion material Li4Ti5O12 from rutile TiO2 via surface activation

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  43. Improvement of the high rate capability of hierarchical structured Li4Ti5O12 induced by the pseudocapacitive effect

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  44. Facile synthesis of hierarchically porous Li4Ti5O12 microspheres for high rate lithium ion batteries

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  45. MnO/C Nanocomposites as High Capacity Anode Materials for Li-Ion Batteries

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  46. Ordered multimodal porous carbon with hierarchical nanostructure for high Li storage capacity and good cycling performance

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  47. Facile synthesis and high rate capability of Li4Ti5O12/C composite materials with controllable carbon content

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  48. Basic molten salt process—A new route for synthesis of nanocrystalline Li4Ti5O12–TiO2 anode material for Li-ion batteries using eutectic mixture of LiNO3–LiOH–Li2O2

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  49. High capacity three-dimensional ordered macroporous CoFe2O4 as anode material for lithium ion batteries

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  50. Solution-Combustion Synthesized Nanocrystalline Li4Ti5O12 As High-Rate Performance Li-Ion Battery Anode

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